Calix[4]- and calix[5]arene-based multicavity macrocycles

被引：19
|
作者：
Notti, A
Occhipinti, S
Pappalardo, S
Parisi, MF
Pisagatti, I
White, AJP
Williams, DJ
机构：
[1] Univ Catania, Dipartimento Sci Chim, I-95125 Catania, Italy
[2] Univ Messina, Dipartimento Chim Organ & Biol, I-98166 Messina, Italy
[3] Imperial Coll Sci Technol & Med, Dept Chem, London SW7 2AY, England
来源：
JOURNAL OF ORGANIC CHEMISTRY | 2002年 / 67卷 / 21期
关键词：
D O I：
10.1021/jo025735w
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Synthesis and single-crystal X-ray structures of mixed triple and double calixarenes 6 and 7, obtained from the base-catalyzed condensation of calix [5] arene 1 with cone pertosylated calix[4]arene 2, are reported. VT-NMR studies on 7 are consistent with a molecular motion arising from the anti-gauche conformational interconversion of its ethylene linkages.
引用
收藏
页码：7569 / 7572
页数：4
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