Synthesis of CuS nanorods by one-step reaction

被引:44
|
作者
Wang, XB
Xu, CQ
Zhang, ZC [1 ]
机构
[1] Univ Sci & Technol China, Dept Polymer Sci & Engn, Hefei 230026, Anhui, Peoples R China
[2] Shizuoka Univ, Innovat Joint Res Ctr, Hamamatsu, Shizuoka 4328561, Japan
关键词
nanorods; solid-state reaction; synthesis;
D O I
10.1016/j.matlet.2005.08.048
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A one-step, solid-state reaction route was developed to synthesize copper sulfide (CuS) nanorods via grinding Cu(NO3)(2)(.)3H(2)O and Na(2)S(.)9H(2)O in existence of ethylenediamine tetraacetic acid disodium salt (Na(2)EDTA-2H(2)O) at ambient temperature. The as-prepared CuS nanorods have diameters of 5 similar to 7 run, lengths up to 40-70 nm. Transmission electron microscopy (TEM) and X-ray diffraction (XRD) were used to characterize the obtained product. A possible reaction mechanism was discussed at the end of this article. (c) 2005 Elsevier B.V. All rights reserved.
引用
收藏
页码:345 / 348
页数:4
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