SnO2/SiO2 Nanocomposite Catalyzed One-Pot Synthesis of 2-Arylbenzothiazole Derivatives

被引:25
|
作者
Yelwande, Ajeet A. [1 ]
Navgire, Madhukar E. [1 ]
Tayde, Deepak T. [1 ]
Arbad, Balasaheb R. [1 ]
Lande, Machhindra K. [1 ]
机构
[1] Dr Babasaheb Ambedkar Marathwada Univ, Dept Chem, Aurangabad 431004, Maharashtra, India
来源
关键词
Nanocomposite; Sol-gel; SnO2/SiO2; Heterogeneous catalyst; 2-Arylbenzothiazoles; SNO2; THIN-FILMS; TIN OXIDE; 2-SUBSTITUTED BENZOTHIAZOLES; HIGHLY EFFICIENT; ACID; NANOPARTICLES; INHIBITORS; REMOVAL;
D O I
10.5012/bkcs.2012.33.6.1856
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
SnO2/SiO2 nanocomposite has been synthesized by using sot-gel method. Prepared catalytic materials has been well characterized by using X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), Fourier transform infrared spectroscopy (FT-IR), Brunauer-Emmer-Teller (BET) surface area, and temperature-programmed desorption of ammonia (NH3-TPD). SnO2/SiO2 nanocomposite catalyzed synthesis of 2-arylbenzothiazoles by the cyclocondensation of 2-aminothiophenol and aromatic aldehydes under reflux condition in 1:1 EtOH:H2O. After completion of the reaction, catalyst can be recovered efficiently and reused with consistent activity.
引用
收藏
页码:1856 / 1860
页数:5
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