Growth and characterization of tris thiourea chromium(III) sulphate

被引：8
|
作者：
Madhurambal, G. [4 ]
Ravindran, B. [3 ]
Mariappan, M. [3 ]
Mojumdar, S. C. [1 ,2 ]
机构：
[1] Univ Guelph, Dept Chem, Guelph, ON N1G 2W1, Canada
[2] Trencin Univ A Dubcek, Fac Ind Technol, Dept Chem Technol & Environm, Puchov 02032, Slovakia
[3] EGS Pillay Engn Coll, Nagapattinam 611002, India
[4] ADM Coll Women, Nagapattinam 611001, India
来源：
JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY | 2012年 / 108卷 / 03期
关键词：
Tris thiourea chromium(III) sulphate; Slow evaporation; UV; FTIR; TG; DTA; COMPLEXES; BEHAVIOR;
D O I：
10.1007/s10973-012-2360-0
中图分类号：
O414.1 [热力学];
学科分类号：
摘要：
Single crystal of tris thiourea chromium(III) sulphate was grown by slow evaporation technique at 303 K. The structural properties of the grown crystals were characterized by FTIR spectroscopy, UV spectroscopy and powder X-ray diffraction analysis. FTIR and UV spectra provide information about the presence of functional groups. Thermal analysis confirms that the crystal is thermally stable up to 163.48 A degrees C. The TG curve presented a two-step mass loss on heating the compound at 0-1,200 A degrees C.
引用
收藏
页码：905 / 910
页数：6
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