New generation of functionalized bipyrazolic tripods: synthesis and study of their coordination properties towards metal cations

被引：23

作者：

Harit, Tarik ^{[2
]}

Cherfi, Mounir ^{[2
]}

Isaad, Jalal ^{[1
]}

Riahi, Abdelkhalek ^{[3
]}

Malek, Fouad ^{[2
]}

机构：

[1] Univ Lille Nord France, Engn & Text Mat Lab, F-5900 Lille, France

[2] Univ Mohamed Premier, Fac Sci, Lab Chim Organ Macromol & Prod Nat URAC 25, Oujda 60000, Morocco

[3] Univ Reims, Inst Chim Mol Reims, Grp Methodol Synth Organ, CNRS UMR 6229, F-51687 Reims 2, France

来源：

TETRAHEDRON | 2012年 / 68卷 / 21期

关键词：

Bipyrazolic tripods; N-Donor; Complexing properties; Coordination; Liquid-liquid extraction; TRANSPORT ABILITIES; LARIAT ETHERS; LIGANDS; DERIVATIVES; COMPLEXES; COPPER; INHIBITORS; STABILITY; CORROSION; SERIES;

D O I：

10.1016/j.tet.2012.03.052

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A simple and easily synthesis of new generation of N-donor bipyrazolic tripods by coupling of functionalized pyrazole derivatives and an appropriate primary amine derivative via condensation or nucleophilic substitution reaction is presented. The complexation capacity of these compounds towards bivalent metal ions (Hg2+, Cu2+, Pb2+, Cd2+) and alkaline metal ions (Li+, Na+, K+) were investigated using the liquid-liquid extraction process. The percentage limits of extraction were determined by atomic absorption measurements. (C) 2012 Elsevier Ltd. All rights reserved.

引用

页码：4037 / 4041

页数：5

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