Preparation and physicochemical study of nickel(II) thiostannate in the NiCl2-SnS2-H2O system

被引：0
|
作者：
Mamedova, N. A. [1 ]
Ragimov, S. S. [1 ]
Sadykhov, F. M. [1 ]
Aliev, I. I. [1 ]
机构：
[1] Natl Acad Sci Azerbaijan, Nagiev Inst Chem Problems, Baku, Azerbaijan
来源：
RUSSIAN JOURNAL OF INORGANIC CHEMISTRY | 2012年 / 57卷 / 02期
关键词：
Physicochemical Study; Chalcogen; Dimethylglyoxime; Ammonium Acetate Buffer Solution; Follow Unit Cell Parameter;
D O I：
10.1134/S0036023612020179
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Nickel(II) thiostannate is prepared in the NiCl2-SnS2-H2O system by precipitation from solutions. Its formation temperature and homogenization time are determined. The synthesis of NiSnS3 from the ammonium acetate buffer solution is found to last 6-8 h at 80-90A degrees C. The elemental composition of ternary nickel(II) thiostannate is detrermined by chemical analysis.
引用
收藏
页码：160 / 162
页数：3
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