Pesticide Analysis in Agricultural Products by GC-MS/MS Using STQ Method

被引:0
|
作者
Okubo, Yoshitsugu [1 ,2 ]
Yagi, Masahiro [1 ]
机构
[1] Kobe Inst Hlth, Chuo Ku, 4-6-5 Minatojima Nakamachi, Kobe, Hyogo 6500046, Japan
[2] North Sanitat Inspect Off, Kobe Publ Hlth Ctr, Kita Ku, 1-9-1 Suzurandai Kitamachi, Kobe, Hyogo 6511114, Japan
来源
FOOD HYGIENE AND SAFETY SCIENCE | 2020年 / 61卷 / 01期
关键词
polymer-based solid-phase extraction mini-column; GC-MS/MS; STQ STQ method; pesticide residue; large-volume injection; stomach-type glass line; SOLID-PHASE EXTRACTION; MULTIRESIDUE METHOD; RESIDUES;
D O I
暂无
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
As a method to detect pesticide residues in agricultural products, we evaluated the pretreatment of agricultural product samples by the solid-phase extracton technique with QuEChERS (STQ) method followed by GC-MS/MS with large-volume injection using a stomach-type glass-lined injector. This method satisfied the target criteria of recovery (70-120%) and the standard deviation of repeatability (RSD < 25%) in 238-282 pesticides found in six types of agricultural products.
引用
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页码:47 / 52
页数:6
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