Preparation and characterization of Pd2Sn nanoparticles

被引：16

作者：

Page, Katharine

Schade, Christina S.

Zhang, Jinping

Chupas, Peter J.

Chapman, Karena W.

Proffen, Thomas

Cheetham, Anthony K.

Seshadri, Ram ^{[1
]}

机构：

[1] Univ Calif Santa Barbara, Dept Mat, Mat Res Lab, Santa Barbara, CA 93106 USA

[2] Johannes Gutenberg Univ Mainz, Inst Anorgan Chem & Analyt Chem, D-55099 Mainz, Germany

[3] Argonne Natl Lab, Adv Photon Source, Argonne, IL 60439 USA

[4] Lujan Neutron Scattering Ctr, LANSCE 12, Los Alamos Natl Lab, Los Alamos, NM 87545 USA

来源：

MATERIALS RESEARCH BULLETIN | 2007年 / 42卷 / 12期

基金：

美国国家科学基金会;

关键词：

intermetallic compounds; electron microscopy; neutron scattering; X-ray diffraction;

D O I：

10.1016/j.materresbull.2007.05.010

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

We report a non-aqueous solution preparation of Pd2Sn nanoparticles with sizes near 20 nm. The intermetallic compound with the Co2Si structure has been characterized using transmission electron microscopy, Rietveld refinement of synchrotron X-ray and neutron powder diffraction, and real-space pair distribution function analysis of high-energy synchrotron X-ray scattering. We also present a description of the electronic structure of this covalent intermetallic using density functional calculations of the electronic structure. (c) 2007 Published by Elsevier Ltd.

引用

页码：1969 / 1975

页数：7

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