The first total synthesis of phebaclavin A and C

被引:2
|
作者
Zhang, Y [1 ]
Liu, D [1 ]
Li, Y [1 ]
Cao, XP [1 ]
机构
[1] Lanzhou Univ, Coll Chem & Chem Engn, State Key Lab Organ Chem, Lanzhou 730000, Peoples R China
关键词
phebaclavin A; phebaclavin C; solvent-free cyclizing reaction; Wittig reaction;
D O I
10.1002/cjoc.200591453
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Phebaclavin A (1) and C (2) were synthesized in 60% and 58% total yields over 5 steps from commercially available starting meterials respectively. The synthesis feature was usage of the Wittig reaction twice and solvent-free cyclizing reaction as the key steps.
引用
收藏
页码:1453 / 1456
页数:4
相关论文
共 50 条
  • [1] The first total synthesis of usabamycins a and C
    Sakaine, Guna
    Zemribo, Ronalds
    Smits, Gints
    TETRAHEDRON LETTERS, 2017, 58 (25) : 2426 - 2428
  • [2] First total synthesis of haplacutine C
    Kutsumura, Noriki
    Numata, Keisuke
    Saito, Takao
    TETRAHEDRON LETTERS, 2016, 57 (50) : 5581 - 5583
  • [3] The first total synthesis of efrapeptin C
    Jost, M
    Greie, JC
    Stemmer, N
    Wilking, SD
    Altendorf, K
    Sewald, N
    ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2002, 41 (22) : 4267 - 4269
  • [4] First total synthesis of bauerine C
    Lingam, Y.
    Rao, D. Muralimohan
    Bhowmik, Dipal R.
    Islam, Aminul
    SYNTHETIC COMMUNICATIONS, 2007, 37 (22-24) : 4313 - 4318
  • [5] First total synthesis of pygmaeocin C
    Liu, HJ
    Chin, CL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2004, 227 : U175 - U175
  • [6] The First Total Synthesis of Synparvolide C
    Sabitha, Gowravaram
    Sandeep, AnkiReddy
    Rao, Allu Senkara
    Yadav, Jhillu S.
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2013, 2013 (29) : 6702 - 6709
  • [7] First total synthesis of Debilisone C
    Saikia, Bishwajit
    Devi, Thongam Joymati
    Barua, Nabin C.
    ORGANIC & BIOMOLECULAR CHEMISTRY, 2013, 11 (06) : 905 - 913
  • [8] First total synthesis of desmosdumotin C
    Nakagawa-Goto, K
    Wu, JH
    Lee, KH
    SYNTHETIC COMMUNICATIONS, 2005, 35 (13) : 1735 - 1739
  • [9] First total synthesis of topopyrone C
    Gattinoni, Sonia
    Merlini, Lucio
    Dallavalle, Sabrina
    TETRAHEDRON LETTERS, 2007, 48 (06) : 1049 - 1051
  • [10] First stereoselective total synthesis of pectinolide C and total synthesis of pectinolide A
    Sabitha, Gowravaram
    Das, Sukant Kishore
    AnkiReddy, Praveen
    Yadav, J. S.
    TETRAHEDRON LETTERS, 2013, 54 (09) : 1097 - 1099