Redetermination of bis[di-n-butylbis(thiophene-2-carboxylato-O,O′)tin(VI) oxide] at low temperature

被引：4
|
作者：
Yahyi, A
Et-touhami, A
Ramdani, A
Benchat, N
El-Bali, B
Bolte, M
机构：
[1] Univ Frankfurt, Inst Organ Chem, D-60439 Frankfurt, Germany
[2] Fac Sci, Chim Organ Phys Lab, Oujda, Morocco
[3] Fac Sci DM, Dept Chim, Lab Mat & Protect Environm, Fes Atlas, Morocco
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2001年 / 57卷
关键词：
D O I：
10.1107/S1600536801004214
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, octa-n-butyl-1 kappa (2) C,2 kappa (2) C,3 kappa (2) C,4 kappa (2) C-di-mu (3) oxo-1:2:3 kappa (3) O;2:3:4:kappa (3) O-tetrakis(thiophene-2-carboxylate)1 kappaO;1:2 kappa (2) O:O';3:4 kappa (2) O:O';4 kappaO-tetratin(VI), [Sn4O2 (C4H9)(8) (C5H3O2S)(4)], contains a planar Sn2O2 ring. The crystal structure is a racemic twin and shows pseudo-centrosymmetry. A previous structure determination of the title compound [Vatsa et al. (1990). J. Organomet. Chem. 396, 9-18] showed the same cell parameters but a centrosymmetric molecule in space group P2(1)/c.
引用
收藏
页码：m148 / m150
页数：3
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