Synthesis and crystal structure of N-(1-phenyl-3-methyl-4-benzal-pyrazolone-5)-furoic hydrazide

被引：0
|
作者：
Liu, L
Ji, YL
Jia, DZ [1 ]
Yu, KB
机构：
[1] Xinjiang Univ, Inst Appl Chem, Urumqi 830046, Peoples R China
[2] Chinese Acad Sci, Chengdu Inst Organ Chem, Chengdu 610012, Peoples R China
来源：
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2003年 / 22卷 / 05期
关键词：
synthesis; crystal structure; furoic hydrazide; pyrazolone;
D O I：
暂无
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
N-(1-Phenyl-3-methyl-4-benzal-pyrazolone-5)-furoic hydrazide (PMBP-FUH, C22H18N4O3, CCDC No: 188946) has been synthesized and characterized by IR spectrum, H-1 NMR and single-crystal X-ray diffraction. The crystal is of orthorhombic, space group Pbca with a = 11.870(2), b = 15.951(3), c = 19.674(3) Angstrom, V = 3725.0(11) Angstrom(3), M-r = 386.40, Z = 8, D-c = 1.378 g/cm(3), F(000) = 1616, R = 0.0455 and wR = 0.0809. The inter- or intramolecular hydrogen bonds result in the formation of three-dimensional network structure.
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页码：568 / 572
页数：5
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