Comparison of solid-phase extraction sorbents for sample clean-up in the analysis of organic explosives

被引：38

作者：

Tachon, Romain ^{[2
]}

Pichon, Valerie ^{[1
]}

Le Borgne, Martine Barbe ^{[2
]}

Minet, Jean-Jacques ^{[2
]}

机构：

[1] Ecole Super Phys & Chim Ind Ville Paris, CNRS, UMR 7121, Lab Environm & Chim Analyt, F-75231 Paris 05, France

[2] Lab Cent Prefecture Police, F-75015 Paris, France

来源：

JOURNAL OF CHROMATOGRAPHY A | 2008年 / 1185卷 / 01期

关键词：

explosives; nitrate esters; nitramines; nitroaromatics; SPE; LC/UV; LC/MS;

D O I：

10.1016/j.chroma.2008.01.026

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A solid-phase extraction procedure was developed for the clean-up of forensic samples collected at bombing scenes. Recoveries of common organic explosives from methanolic extracts diluted with water were studied on different hydrophobic sorbents. Polymeric sorbents retained explosive compounds better than octadecyl-bonded silica-bascd materials. Clean-up efficiency was evaluated with simulated samples prepared from commercial motor oil. Polymeric sorbent with the smallest specific surface area was found to limit the coextraction of matrix components. Performance of the method was confirmed by a reduction of ion suppression in LC/MS analysis. (C) 2008 Published by Elsevier B.V.

引用

页码：1 / 8

页数：8

共 50 条

[1] Systematic Comparison of Extract Clean-Up with Currently Used Sorbents for Dispersive Solid-Phase Extraction
Peter, Michelle
Mueller, Christoph
MOLECULES, 2024, 29 (19):
[2] Solid-phase extraction clean-up procedure for the analysis of PAHs in lichens
Blasco, Maria
Domeno, Celia
Bentayeb, Karim
Nerin, Cristina
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 2007, 87 (12) : 833 - 846
[3] Optimization of solid phase extraction technique for a sample clean-up procedure
Matyska, M. T.
Siouffi, A. M.
Volpe, N.
Chemia Analityczna, 40 (01):
[4] Improved extraction and clean-up of imidazolinone herbicides from soil solutions using different solid-phase sorbents
Ramezani, Mohammadkazem
Simpson, Nigel
Oliver, Danielle
Kookana, Rai
Gill, Gurjeet
Preston, Christopher
JOURNAL OF CHROMATOGRAPHY A, 2009, 1216 (26) : 5092 - 5100
[5] Suitability testing of commercial solid-phase extraction sorbents for sample clean-up in systematic toxicological analysis using liquid chromatography-(tandem) mass spectrometry
Decaestecker, TN
Coopman, EM
Van Peteghem, CH
Van Bocxlaer, JF
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES, 2003, 789 (01): : 19 - 25
[6] Comparison of commercial solid-phase extraction sorbents for the sample preparation of potato glycoalkaloids
Väänänen, T
Kuronen, P
Pehu, E
JOURNAL OF CHROMATOGRAPHY A, 2000, 869 (1-2) : 301 - 305
[7] Graphene Adsorbent-Based Solid-Phase Extraction for Aflatoxins Clean-Up in Food Samples
Feizy, Javad
Jahani, Moslem
Beigbabaei, Adel
CHROMATOGRAPHIA, 2019, 82 (06) : 917 - 926
[8] Graphene Adsorbent-Based Solid-Phase Extraction for Aflatoxins Clean-Up in Food Samples
Javad Feizy
Moslem Jahani
Adel Beigbabaei
Chromatographia, 2019, 82 : 917 - 926
[9] Determination of organochlorine pesticide residues in foods using solid-phase extraction clean-up cartridges
Doong, RA
Lee, CY
ANALYST, 1999, 124 (09) : 1287 - 1289
[10] Analysis of polycyclic aromatic hydrocarbons in vegetable oils combining gel permeation chromatography with solid-phase extraction clean-up
Fromberg, A.
Hojgard, A.
Duedahl-Olesen, L.
FOOD ADDITIVES AND CONTAMINANTS PART A-CHEMISTRY ANALYSIS CONTROL EXPOSURE & RISK ASSESSMENT, 2007, 24 (07): : 758 - 767

← 1 2 3 4 5 →