Nano-sized Fe-metal catalyst on ZnO-SiO2: (photo-assisted deposition and impregnation) Synthesis routes and nanostructure characterization

被引：20

作者：

Mohamed, R. M. ^{[1
,2
]}

Al-Rayyani, M. A. ^{[1
]}

Baeissa, E. S. ^{[1
]}

Mkhalid, I. A. ^{[1
]}

机构：

[1] King Abdulaziz Univ, Fac Sci, Dept Chem, Jeddah 21589, Saudi Arabia

[2] CMRDI, Adv Mat Dept, Cairo, Egypt

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2011年 / 509卷 / 24期

关键词：

Sol-gel technique; Visible photocatalyst; Waste water treatment; PHOTOCATALYTIC DEGRADATION; METHYLENE-BLUE; ZNO; SILICA;

D O I：

10.1016/j.jallcom.2011.03.098

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

A nano-sized Fe metal on ZnO-SiO2 was synthesized using the photo-assisted deposition (PAD) and impregnation routes. The obtained samples were characterized by a series of techniques including X-ray diffraction (XRD), UV-vis diffuse reflectance spectroscopy, N-2 adsorption, extended X-ray absorption fine structure (EXAFS), and transmission electron microscopy (TEM). Photocatalytic reactivity using Fe-ZnO-SiO2 catalysts under visible-light condition on the degradation of methylene blue dye was evaluated. The results of characterization reveal, a notable photocatalytic activity of PAD:Fe-ZnO-SiO2 which was about 9 and 12 times higher than that of Img:Fe-ZnO-SiO2 and ZnO-SiO2, respectively. (C) 2011 Elsevier B.V. All rights reserved.

引用

页码：6824 / 6828

页数：5

共 20 条

[1] Nano-sized Fe-Metal Catalyst on TiO2-SiO2: (Photo-assisted Deposition and Impregnation) Synthesis Routes and Nanostructure Characterization
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ASIAN JOURNAL OF CHEMISTRY, 2013, 25 (16) : 8887 - 8891
[2] Characterization and catalytic properties of nano-sized Ag metal catalyst on TiO2-SiO2 synthesized by photo-assisted deposition and impregnation methods
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[3] Characterization and catalytic properties of nano-sized Pt metal catalyst on TiO2-SiO2 synthesized by photo-assisted deposition and impregnation methods
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[4] A new application of photocatalysts: synthesis of nano-sized metal and alloy catalysts by a photo-assisted deposition method
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[5] A new application of photocatalysts: synthesis of nano-sized metal and alloy catalysts by a photo-assisted deposition method
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[8] Characterization and Catalytic Properties of Nano-Sized AuMetal Catalyst on Titanium Containing High Mesoporous Silica (Ti-HMS) Synthesized by Photo-Assisted Deposition and Impregnation Methods
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[9] XAFS study on nano-sized pd metal catalyst deposited on ti-containing zeolite by a photo-assisted deposition (PAD) method
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[10] Preparation of nano-sized platinum metal catalyst using photo-assisted deposition method on mesoporous silica including single-site photocatalyst
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