Three Cu(II) Complexes Constructed by Flexible bis-Imidazole and Different Anions: From 0D Architecture to 2D Layer

被引：3
|
作者：
Lu, J. F. [1 ]
Yu, X. H. [1 ]
Zhao, C. B. [1 ]
Zheng, N. [1 ]
Yue, S. Y. [1 ]
Li, L. [1 ]
Tang, Z. H. [1 ]
Ge, H. G. [1 ]
Jin, L. X. [1 ]
机构：
[1] Shaanxi Univ Technol, Coll Chem & Environm Sci, Shaanxi Key Lab Catalysis, Hanzhong 723001, Peoples R China
来源：
CRYSTALLOGRAPHY REPORTS | 2019年 / 64卷 / 07期
基金：
中国国家自然科学基金;
关键词：
METAL-ORGANIC FRAMEWORKS; CRYSTAL-STRUCTURE; POROUS MATERIAL;
D O I：
10.1134/S1063774519070095
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Three new Cu(II) complexes, Cu(1,3-bip)(Ac)(2) (I), {[Cu(H2O)(2)(1,3-bip)(2)] center dot (NO3)(2)}(n) (II), {[Cu(1,3-bip)(1,4-bdc)](2) center dot H2O center dot MeOH}(n) (III), where 1,3-bip is 1,3-bis(imidazole)propane and 1,4-bdc is terephthalic acid, have been synthesized and characterized by single crystal and powder X-ray diffraction, Fourier transform infrared spectroscopy, and elemental analysis. Single crystal X-ray diffraction reveals that the complex I shows a zero-dimensional architecture, the complex II shows a one-dimensional loop-like chain, and the complex III shows a two-dimensional (4,4) grid layer structure. In addition, the thermal stability of complexes was investigated.
引用
收藏
页码：1055 / 1061
页数：7
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