In situ analysis of electrocrystallization process of metal electrodeposition with confocal energy dispersive X-ray diffraction based on polycapillary X-ray optics

被引：7
|
作者：
Li, Fangzuo [1 ,2 ,3 ]
Liu, Zhiguo [1 ,2 ,3 ]
Sun, Tianxi [1 ,2 ,3 ]
Yang, Chaolin [1 ,2 ,3 ]
Sun, Weiyuan [1 ,2 ,3 ]
Sun, Xuepeng [1 ,2 ,3 ]
Ma, Yongzhong [4 ]
Ding, Xunliang [1 ,2 ,3 ]
机构：
[1] Beijing Normal Univ, Minist Educ, Key Lab Beam Technol & Mat Modificat, Beijing 100875, Peoples R China
[2] Beijing Normal Univ, Coll Nucl Sci & Technol, Beijing 100875, Peoples R China
[3] Beijing Radiat Ctr, Beijing 100875, Peoples R China
[4] Ctr Dis Control & Prevent Beijing, Beijing 100013, Peoples R China
来源：
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT | 2015年 / 785卷
基金：
中国国家自然科学基金;
关键词：
Polycapillary X-ray optics; Confocal energy dispersive X-ray diffraction; Electrocrystallization; In situ real-time analysis; THIN-FILMS; GROWTH; COPPER; NUCLEATION; FLUORESCENCE; SYSTEM; EDXRD; RECRYSTALLIZATION; CRYSTALLIZATION; KINETICS;
D O I：
10.1016/j.nima.2015.03.015
中图分类号：
TH7 [仪器、仪表];
学科分类号：
0804 ; 080401 ; 081102 ;
摘要：
The confocal energy dispersive X-ray diffraction (EDXRD) based on a polycapillary focusing X-ray lens (PFXRL) in excitation channel and a polycapillary parallel X-ray lens (PPXRL) in detection channel was presented to study the electrocrystallization process of metal electrodeposition. The input focal spot of the PPXRL and the output focal spot of the PFXRL was adjusted in a confocal configuration, and only the X-rays from the volume overlapped by the two foci could be accordingly detected by the detector. The experimental results demonstrated the confocal EDXRD could be used to in situ real-time analysis of electrochemical crystal growth process. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码：201 / 205
页数：5
相关论文
共 50 条
  • [1] Micro Energy Dispersive X-Ray Diffraction Analysis by Polycapillary X-Ray Optics Focusing
    Duan Zeming
    Jiang Qili
    Liu Jun
    Pan Qiuli
    Cheng Lin
    [J]. ACTA OPTICA SINICA, 2018, 38 (12)
  • [2] Performances for confocal X-ray diffraction technology based on polycapillary slightly focusing X-ray optics
    Liu, Hehe
    Liu, Zhiguo
    Sun, Tianxi
    Peng, Song
    Ma, Yongzhong
    Sun, Weiyuan
    Li, Yude
    Lin, Xiaoyan
    Zhao, Weigang
    Zhao, Guangcui
    Luo, Ping
    Pan, Qiuli
    Ding, Xunliang
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2013, 723 : 1 - 4
  • [3] Performance of polycapillary X-ray optics for confocal energy-dispersive small-angle X-ray scattering
    Sun, Tianxi
    Peng, Song
    Liu, Zhiguo
    Sun, Weiyuan
    Ma, Yongzhong
    Ding, Xunliang
    [J]. JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2013, 46 : 1880 - 1883
  • [4] Polycapillary optics for energy dispersive micro x-ray diffractometry
    Bjeoumikhov, A
    Bjeoumikhova, S
    Langhoff, N
    Wedell, R
    [J]. APPLIED PHYSICS LETTERS, 2005, 86 (14) : 1 - 3
  • [5] Measurement of grain size of polycrystalline materials with confocal energy dispersive micro-X-ray diffraction technology based on polycapillary X-ray optics
    [J]. Sun, T. (stx@bnu.edu.cn), 1600, Elsevier B.V., Netherlands (764):
  • [6] Measurement of grain size of polycrystalline materials with confocal energy dispersive micro-X-ray diffraction technology based on polycapillary X-ray optics
    Sun, Weiyuan
    Liu, Zhiguo
    Sun, Tianxi
    Peng, Song
    Ma, Yongzhong
    Li, Fangzuo
    Sun, Xuepeng
    Ding, Xunliang
    [J]. NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT, 2014, 764 : 1 - 6
  • [7] Time-Resolved x-ray diffraction with polycapillary x-ray optics
    Gao, Y.
    DeCamp, M. F.
    [J]. 2011 CONFERENCE ON LASERS AND ELECTRO-OPTICS (CLEO), 2011,
  • [8] Development of Polycapillary X-ray Optics for X-Ray Spectroscopy
    Adams, Bernhard W.
    Attenkofer, Klaus
    Bond, Justin L.
    Craven, Christopher A.
    Cremer, Till
    O'Mahony, Aileen
    Minot, Michael J.
    Popecki, Mark A.
    [J]. ADVANCES IN LABORATORY-BASED X-RAY SOURCES, OPTICS, AND APPLICATIONS V, 2016, 9964
  • [9] Full-field transmission x-ray imaging with confocal polycapillary x-ray optics
    Sun, Tianxi
    MacDonald, C. A.
    [J]. JOURNAL OF APPLIED PHYSICS, 2013, 113 (05)
  • [10] Experimental Qualification of a Novel X-Ray Diffraction Imaging Setup Based on Polycapillary X-Ray Optics
    Castoldi, A.
    Ozkan, C.
    Guazzoni, C.
    Bjeoumikhov, A.
    Hartmann, R.
    [J]. IEEE TRANSACTIONS ON NUCLEAR SCIENCE, 2010, 57 (05) : 2564 - 2570
12345