Preparation and characterization of nanometer titania-coated silica particles

被引:0
|
作者
Ma, YL [1 ]
Zhu, HL
Wang, Y
机构
[1] Tianjin Univ, Inst Sci, Dept Chem, Tianjin 300072, Peoples R China
[2] Mengguli Power Supply Technol Ltd Co, Beijing 102200, Peoples R China
关键词
nanometer TiO2-coated silica particles; microemulsion technology; sol-gel process; chemical bond;
D O I
暂无
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Silica gel particles prepared by microemulsion technology were used as the corns, which were subsequently coated nanometer titania layer through sol-gel process. Phase compositions and microstructures of nanometer TiO2-coated silica particles were characterized. The results of experiments indicate that the size of nanometer TiO2-coated silica particles is about 250nm. The coated-TiO2 layers with the average thickness of 20 nm similar to 40nm are uniform. With the calcining temperature rising from 550 degrees C to 850 degrees C, the coated-TiO2 layers indicate anatase-phase crystal structure, and the size of nanometer titania in the coated-layers is less than 20nm. The Ti-O-Si chemical bond is formed at the corn-layer interfaces confirmed by XPS and FT-IR.
引用
收藏
页码:174 / 177
页数:4
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