Gradient thin-layer chromatography and densitometry determination of Alternaria mycotoxins

被引:18
|
作者
Matysik, G [1 ]
Giryn, H [1 ]
机构
[1] INST BIOTECHNOL AGR & FOOD IND, PL-02532 WARSAW, POLAND
关键词
thin-layer chromatography; stepwise gradient elution; Alternaria; mycotoxins in food;
D O I
10.1007/BF02290291
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Mycotoxins produced by the genus Alternaria in cereals, tomatoes and raspberries were analysed by stepwise gradient thin-layer chromatography (HPTLC plates). The chromatograms were suitable for direct quantitative densitometric determination of alternariotoxins. Extraction of samples was with ethyl acetate. Extracts of were purified on glass columns of silica gel Si 60 for column chromatography.
引用
下载
收藏
页码:555 / 558
页数:4
相关论文
共 50 条
  • [1] DETERMINATION OF HYPERICIN AND PSEUDOHYPERICIN BY THIN-LAYER CHROMATOGRAPHY DENSITOMETRY
    KARTNIG, T
    GOBEL, I
    JOURNAL OF CHROMATOGRAPHY, 1992, 609 (1-2): : 423 - 426
  • [2] Thin-layer chromatography/densitometry
    Sherma, J
    JOURNAL OF AOAC INTERNATIONAL, 2000, 83 (06) : 1455 - 1455
  • [3] STEPWISE GRADIENT THIN-LAYER CHROMATOGRAPHY AND DENSITOMETRY OF PREDNISOLONE ACETATE
    MATYSIK, G
    TOCZOLOWSKI, J
    MATYSIK, A
    CHROMATOGRAPHIA, 1995, 40 (11-12) : 737 - 739
  • [4] THIN-LAYER CHROMATOGRAPHY OF MYCOTOXINS
    BETINA, V
    JOURNAL OF CHROMATOGRAPHY, 1985, 334 (03): : 211 - 276
  • [5] Determination of biogenic amines in wine by thin-layer chromatography/densitometry
    Romano, Andrea
    Klebanowski, Herve
    La Guerche, Stephane
    Beneduce, Luciano
    Spano, Giuseppe
    Murat, Marie-Laure
    Lucas, Patrick
    FOOD CHEMISTRY, 2012, 135 (03) : 1392 - 1396
  • [6] Determination of New Antidepressants in Pharmaceuticals by Thin-Layer Chromatography with Densitometry
    Gondova, Tatana
    Petrikova, Iveta
    JOURNAL OF AOAC INTERNATIONAL, 2010, 93 (03) : 778 - 782
  • [7] Thin-layer chromatography-densitometry
    Sherma, J
    JOURNAL OF AOAC INTERNATIONAL, 2005, 88 (05) : 1516 - 1516
  • [8] Quantitative determination of pesticides in soil by thin-layer chromatography and video densitometry
    Petrovic, M
    Babic, S
    Kastelan-Macan, M
    CROATICA CHEMICA ACTA, 2000, 73 (01) : 197 - 207
  • [9] DETERMINATION OF POLYOXYETHYLENE NONIONIC SURFACTANTS BY THIN-LAYER CHROMATOGRAPHY AND SPOT DENSITOMETRY
    FAVRETTO, L
    PERTOLDI.G
    FAVRETTO, L
    ANNALI DI CHIMICA, 1972, 62 (7-8) : 478 - 488
  • [10] Phospholipids determination in vegetable oil by thin-layer chromatography and imaging densitometry
    Nzai, JM
    Proctor, A
    FOOD CHEMISTRY, 1998, 63 (04) : 571 - 576