Sublimation of volatile components of electrolessly reduced Ni-B alloys: Kinetics and mass spectrometry

被引：2
|
作者：
Arslambekov, VA
Petrov, VS
Ivanov, MV
机构：
[1] Russian Acad Sci, Inst Phys Chem, Moscow 117915, Russia
[2] Moscow State Inst Elect & Math, Moscow 109028, Russia
来源：
PROTECTION OF METALS | 2001年 / 37卷 / 04期
基金：
俄罗斯基础研究基金会;
关键词：
Oxidation; Mass Spectrometry; Inorganic Chemistry; Boron; Thermogravimetry;
D O I：
10.1023/A:1010487124674
中图分类号：
TF [冶金工业];
学科分类号：
0806 ;
摘要：
The composition of volatile compounds sublimating at 20-700 degreesC from electrolessly plated Ni-B alloys containing 6.2, 19.6, or 20.8% of boron and either freshly-deposited or subsequently-oxidized, as well as the kinetics of the sublimation, is studied by a precise thermogravimetry technique with an automatic vacuum microbalance combined with a quadrupole mass-spectrometer. The effect of the sublimation on the kinetics of the high-temperature oxidation of the alloys is also investigated. Boron oxides and water mainly sublimate from all the alloys; concurrently, NiB3 also sublimates from fresh deposits at a temperature higher than 600 degreesC.
引用
收藏
页码：327 / 330
页数：4
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