Ni-Biurea complex anchored onto MCM-41: As an efficient and recyclable nanocatalyst for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones

被引：29
|
作者：
Batmani, Hana [1 ]
Pesyan, Nader Noroozi [1 ]
Havasi, Forugh [2 ]
机构：
[1] Urmia Univ, Dept Organ Chem, Fac Chem, Orumiyeh 57159, Iran
[2] Univ Kurdistan, Dept Chem, Fac Sci, POB 66315-416, Sanandaj, Iran
来源：
MICROPOROUS AND MESOPOROUS MATERIALS | 2018年 / 257卷
关键词：
Ni-Biurea complex; MCM-41; Nanocatalyst; 2,3-Dihydroquinazolin-4(1H)-one; SOLVENT-FREE CONDITIONS; HETEROGENEOUS CATALYST; MESOPOROUS SILICA; FACILE SYNTHESIS; DERIVATIVES; ACID; 2-SUBSTITUTED-2,3-DIHYDRO-4(1H)-QUINAZOLINONES; NANOPARTICLES; TRIFLATE; WATER;
D O I：
10.1016/j.micromeso.2017.08.024
中图分类号：
O69 [应用化学];
学科分类号：
081704 ;
摘要：
Ni-Biurea complex supported on functionalized MCM-41 was prepared by a post-grafting method and used as an efficient, recoverable and thermally stable nanocatalyst for the one-pot synthesis of 2,3-dihydroquinazolin-4(1H)-ones from 2-aminobenzamide and aromatic aldehydes in PEG. This nano catalyst was characterized using FT-IR, XRD, SEM, TGA, EDS, ICP and BET techniques. The heterogeneous catalyst showed good recyclability and can be reused for five consecutive cycles without significant loss of its catalytic activity. (C) 2017 Elsevier Inc. All rights reserved.
引用
收藏
页码：27 / 34
页数：8
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