Ejector-based nanoparticle sampling from pressures down to 20 mbar

被引:2
|
作者
Rosenberger, Thore [1 ]
Neises, Julian [1 ]
Kiesler, Dennis [1 ]
Kruis, Frank Einar [1 ]
机构
[1] Univ Duisburg Essen, Ctr Nanointegrat Duisburg Essen CENIDE, Inst Technol Nanostruct NST, D-47057 Duisburg, Germany
关键词
Low-pressure sampling; Particle losses in critical orifices; Online measurements; Continuous sampling; AEROSOL-PARTICLES; SILICON NANOPARTICLES; SIZE; PERFORMANCE; OPERATION; ORIFICE;
D O I
10.1016/j.jaerosci.2020.105531
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
The application of standard online instrumentation, such as scanning mobility particle sizer (SMPS), centrifugal particle mass analyzer or aerosol particle mass analyzer (CPMA/APM), and electrical low-pressure impactor (ELPIthorn) to low-pressure processes is only possible with extensive modification of the devices and extensive calibrations. A low-pressure ejector is a suitable device to transfer aerosol nanoparticles from low-pressure regions to atmospheric pressure and allows the direct use of standard online instrumentation. In this work, a commercial low-pressure ejector is investigated in the pressure range from 20-180 mbar with fully-sintered and size-selected nanoparticles (15-80 nm) in order to extend the application range of online instruments to low-pressure processes and open up a new variety of analysis methods. Results are compared to our previous work which was limited to pressures above 120 mbar. A change in particle size during the measurements for fully-sintered silver particles was not observed. A particle dilution factor between 60-6500 was found. High particle losses in the ejector for large particle sizes are compensated by a lower gas dilution factor.
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页数:8
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