A mechanochemical strategy for IRMOF assembly based on pre-designed oxo-zinc precursors

被引：115

作者：

Prochowicz, D. ^{[1
]}

Sokolowski, K. ^{[2
]}

Justyniak, I. ^{[2
]}

Kornowicz, A. ^{[1
]}

Fairen-Jimenez, D. ^{[3
]}

Friscic, T. ^{[4
,5
]}

Lewinski, J. ^{[1
,2
]}

机构：

[1] Warsaw Univ Technol, Dept Chem, PL-00664 Warsaw, Poland

[2] Polish Acad Sci, Inst Phys Chem, PL-01224 Warsaw, Poland

[3] Univ Cambridge, Dept Chem Engn & Biotechnol, Cambridge CB2 3RA, England

[4] McGill Univ, Dept Chem, Montreal, PQ H3A 0B8, Canada

[5] McGill Univ, FRQNT Ctr Green Chem & Catalysis, Montreal, PQ H3A 0B8, Canada

来源：

CHEMICAL COMMUNICATIONS | 2015年 / 51卷 / 19期

关键词：

METAL-ORGANIC FRAMEWORKS; SOLVENT-FREE SYNTHESIS; ADSORPTION; MOFS; CARBOXYLATES; CONSTRUCTION; REACTIVITY; COMPLEXES; SORPTION; CAPTURE;

D O I：

10.1039/c4cc09917f

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

We demonstrate a mechanochemical strategy that allowed the first successful mechanosynthesis of IRMOFs based on an oxo-centred secondary building unit (SBU). The presented study indicates that controlling the acid-base relationship between reagents is key to mechanochemical synthesis of IRMOFs, revealing a pre-assembled oxo-zinc amidate cluster as an efficient precursor for IRMOF mechanosynthesis.

引用

页码：4032 / 4035

页数：4

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