(S,Sp)-2-[4-(1-methylethyl)-4,5-dihydro-oxazol-1-yl]ferrocenecarboxylic acid

被引：1
|
作者：
Stepnicka, P [1 ]
Císarová, I [1 ]
机构：
[1] Charles Univ Prague, Fac Sci, Dept Inorgan Chem, Prague 12840 2, Czech Republic
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2004年 / 60卷
关键词：
D O I：
10.1107/S1600536804002685
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Chiral oxazolinyl-modified ferrocenecarboxylic acid, (S,S p)-[Fe{η5-C5H3(CO 2H-1)(C6H10NO-2)}(η5-C 5H5)] or [Fe(C5H5)-(C 12H14NO3)], crystallizes as a molecular compound, featuring an intramolecular O-H⋯N hydrogen bond between the carboxyl hydroxy group and oxazoline N atom, with an O⋯N separation of 2.559 (3) Å. The ferrocene substituants are rotated only slightly from the plane of their parent cyclopentadienyl ring: 7.65 (17) (oxazoline) and 2.3 (3)° (carboxyl). © 2004 International Union of Crystallography Printed in Great Britain - all rights reserved.
引用
收藏
页码：M288 / M290
页数：3
相关论文
共 50 条
  • [1] (S)-(+)-2-[ 2-(Biphenyl-2-yl)-1-methylethyl]4,5-dihydro-1H-imidazolium hydrogen oxalate
    Giannella, M
    Gentili, F
    Bruni, B
    Messori, L
    Di Vaira, M
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2005, 61 : O2376 - O2378
  • [2] 2-[4-(4,5-Dihydro-1H-pyrrol-2-yl)phenyl]-4,5-dihydro-1H-imidazole
    Kia, Reza
    Fun, Hoong-Kun
    Kargar, Hadi
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2406 - U2996
  • [3] 4-[2,4,6-tris(1-methylethyl)benzoyl]benzoic acid (S)-(-)-proline
    Fu, TY
    Scheffer, JR
    Trotter, J
    [J]. ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1997, 53 : 1259 - 1262
  • [4] 4-[2,4,6-Tris(1-methylethyl)benzoyl]benzoic acid (S)-(-)-proline
    Fu, Tai Y.
    Scheffer, John R.
    Trotter, James
    [J]. Acta Crystallographica, Section C: Crystal Structure Communications, 1998, C53 (Pt 9): : 1259 - 1262
  • [5] 2-(4,5-Dihydro-1,3-oxazol-2-yl)quinoline
    Machado, Pablo
    Rosa, Fernanda A.
    da Silva, Rubia M. S.
    Burrow, Robert A.
    Martins, Marcos A. P.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O154 - U3891
  • [6] Synthesis and Characterization of Novel 2-(1,2,3-Triazol-4-yl)-4,5-dihydro-1H-pyrazol-1-yl)thiazoles and 2-(4,5-Dihydro-1H-pyrazol-1-yl)-4-(1H-1,2,3-triazol-4-yl)thiazoles
    Kariuki, Benson M.
    Abdel-Wahab, Bakr F.
    Mohamed, Hanan A.
    Bekheit, Mohamed S.
    El-Hiti, Gamal A.
    [J]. MOLECULES, 2022, 27 (24):
  • [7] 2-[4-(4,5-Dihydro-1H-imidazol-2-yl)phenyl]-4,5-dihydro-1H-imidazol-3-ium 4-aminobenzoate
    Song, Xiu-Mei
    Li, Jun-Jun
    Liu, Xin-Hua
    Ren, Chun-Xia
    Shang, Shao-Ming
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O179 - U2936
  • [8] Crystal structure of 2-(1-methylethyl)-1,3-thiazolo[4,5-b]pyridine
    El-Hiti, Gamal A.
    Smith, Keith
    Hegazy, Amany S.
    Alanazi, Saud A.
    Kariuki, Benson M.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : O272 - U222
  • [9] Antibacterial activity studies of 2-[[4-(1-methylethyl) phenyl] methylene]-hydrazinecarboxamide in Escheria coli
    Fernandez, Kelly
    Munguia, Teresita
    [J]. ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2017, 253
  • [10] DETERMINATION OF IMAZAMOX ((2-[4,5-DIHYDRO-4-METHYL-4-(1-METHYLETHYL)-5-OXO-1 H-IMIDAZOL-2-YL]-5-(METHOXYMETHYL)-3-PYRIDINECARBOXYLIC ACID) RESIDUE ON SUNFLOWER PLANT COMPONENTS
    Cebi, U. Kamburoglu
    Ozcan, C.
    Gurbuz, M. A.
    Ozer, S.
    [J]. JOURNAL OF ENVIRONMENTAL PROTECTION AND ECOLOGY, 2019, 20 (01): : 177 - 187
12345