Preparation of ordered mesoporous carbon membranes by a soft-templating method

被引：52
|
作者：
Tanaka, Shunsuke [1 ,2 ]
Nakatani, Norihito [1 ]
Doi, Anna [1 ]
Miyake, Yoshikazu [1 ,2 ]
机构：
[1] Kansai Univ, Fac Environm & Urban Engn, Dept Chem Energy & Environm Engn, Suita, Osaka 5648680, Japan
[2] Kansai Univ, High Technol Res Ctr, Suita, Osaka 5648680, Japan
来源：
CARBON | 2011年 / 49卷 / 10期
基金：
日本学术振兴会;
关键词：
SILICA MEMBRANES; FILMS; FABRICATION;
D O I：
10.1016/j.carbon.2011.03.042
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
Preparation of continuous mesoporous carbon membranes without the use of an intermediate inorganic template was achieved using a thermosetting phenolic resin, resorcinol/phloroglucinol/formaldehyde, and a thermally-decomposable organic template, Pluronic F127 (PEO(106)-PPO(70)-PEO(106)). The coating solution was cast on porous alpha-alumina supports by dip-coating. Afterwards, decomposition of the organic template and solidification of the carbon precursors are simultaneously performed through a carbonization process. A composite layer of carbon/alumina was formed. The single gas permeation was governed by the Knudsen diffusion mechanism. The membrane exhibited high hydrothermal stability and high alkaline resistance. (C) 2011 Elsevier Ltd. All rights reserved.
引用
收藏
页码：3184 / 3189
页数：6
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