Synthesis and characterization of new thiadiazole derivatives bearing a pyrazole moiety

被引：3
|
作者：
Sacmaci, Mustafa [1 ]
Arslaner, Ciler [1 ]
Sahin, Ertan [2 ]
机构：
[1] Bozok Univ, Fac Arts & Sci, Dept Chem, Yozgat, Turkey
[2] Ataturk Univ, Fac Sci, Dept Chem, Erzurum, Turkey
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2017年 / 192卷 / 10期
关键词：
Thiadiazole; pyrazole; X-ray structure; ACID;
D O I：
10.1080/10426507.2017.1345905
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A series of thidiazole derivatives (4, 7) from pyrazole-3-carboxylic acid chloride (2) and pyrazole-3,4-dicarboxylicacid chloride derivatives (6) were synthesized and characterized. The structures of the new compounds were confirmed byelemental analysis, NMR (H-1 and C-13) and IR spectra. The molecular and crystal structure of 4-benzoyl-N-[5-(methylthio)-1,3,4-thiadiazol-2-yl]-1,5-di-phenyl-1H-pyrazole-3carboxamide(4d)was determined by single crystal X-ray diffraction method.
引用
收藏
页码：1134 / 1139
页数：6
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