Microwave-assisted Extraction of Spruce Bark: Statistical Optimization Using Box-Behnken Design

被引：2
|
作者：
Sladkova, Alexandra [1 ]
Stopka, Jan [2 ]
Haz, Ales [1 ]
Strizincova, Petra [1 ]
Surina, Igor [1 ]
Kreps, Frantisek [3 ]
Burcova, Zuzana [3 ]
Jablonsky, Michal [1 ]
机构：
[1] Slovak Univ Technol Bratislava, Fac Chem & Food Technol, Inst Nat & Synthet Polymers, Dept Wood Pulp & Paper, Radlinskeho 9, Bratislava 81237, Slovakia
[2] Slovak Univ Technol Bratislava, Fac Chem & Food Technol, Inst Chem & Environm Engn, Dept Chem & Biochem Engn, Radlinskeho 9, Bratislava 81237, Slovakia
[3] Slovak Univ Technol Bratislava, Fac Chem & Food Technol, Inst Food Sci & Nutr, Dept Food Technol, Radlinskeho 9, Bratislava 81237, Slovakia
来源：
BIORESOURCES | 2018年 / 13卷 / 04期
关键词：
Extraction; Microwave extraction; Spruce bark; Extractives; PICEA-ABIES BARK; ULTRASOUND; POLYPHENOLS; PLANT;
D O I：
10.15376/biores.13.4.8993-9004
中图分类号：
TB3 [工程材料学]; TS [轻工业、手工业、生活服务业];
学科分类号：
0805 ; 080502 ; 0822 ;
摘要：
Closed-system microwave-assisted extraction was applied to extract constituents from spruce bark, using 96.6% ethanol as an extractant. The influence of the time (1 min to 20 min), temperature (60 degrees C, 80 degrees C, and 100 degrees C), and liquid/solid ratio (8 mL/g dry bark to 12 mL/g dry bark) on the yield of extractives was studied. The effects of all three of the factors were explained. The results revealed that the optimum conditions were a liquid/solid ratio of 12.0 mL/g dry bark, extraction temperature of 100 degrees C, and extraction time of 13.4 min.
引用
收藏
页码：8993 / 9004
页数：12
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