A simple microwave-assisted decomposing route for synthesis of ZnO nanorods in the presence of PEG400

被引:55
|
作者
Liu, Jin-song [1 ]
Cao, Jie-ming [1 ]
Li, Zi-quan [1 ]
Ji, Guang-bin [1 ]
Zheng, Ming-bo [1 ]
机构
[1] Nanjing Univ Aeronaut & Astronaut, Coll Mat Sci & Technol, Nanomat Res Inst, Nanjing 210016, Peoples R China
基金
中国国家自然科学基金;
关键词
microwave-assisted decomposing; ZnO nanorods; nanomaterial; optical materials and properties;
D O I
10.1016/j.matlet.2007.02.014
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In the paper, a simple microwave-assisted decomposing reaction in the presence of PEG400 has been successfully developed to synthesize ZnO nanorods with 10-25 nm of diameter and 60-200 mn of length. The product was analyzed and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and HRTEM. Ultraviolet-visible (UV-vis) absorption peak of ZnO nanorods shows a distinct blue shift from that of the bulk and the Photolummescence (PL) spectrum exhibits a strong near-band-edge emission at 385 run. Further experiments have also been designed, and the results show that microwave radiation and surfactant PEG400 all played an important role on the formation of ZnO nanorods. (C) 2007 Published by Elsevier B.V.
引用
收藏
页码:4409 / 4411
页数:3
相关论文
共 50 条
  • [1] Conventional and microwave-assisted synthesis of ZnO nanorods and effects of PEG400 as a surfactant on the morphology
    Erten-Ela, Sule
    Cogal, Sadik
    Icli, Siddik
    [J]. INORGANICA CHIMICA ACTA, 2009, 362 (06) : 1855 - 1858
  • [2] Microwave-Assisted Synthesis of Quinoxalines in PEG-400
    Zhang, Xia-Zhong
    Wang, Jin-Xian
    Bai, Lin
    [J]. SYNTHETIC COMMUNICATIONS, 2011, 41 (14) : 2053 - 2063
  • [3] Microwave-assisted hydrothermal synthesis and characterization of ZnO nanorods
    Ocakoglu, K.
    Mansour, Sh. A.
    Yildirimcan, S.
    Al-Ghamdi, Ahmed A.
    El-Tantawy, F.
    Yakuphanoglu, F.
    [J]. SPECTROCHIMICA ACTA PART A-MOLECULAR AND BIOMOLECULAR SPECTROSCOPY, 2015, 148 : 362 - 368
  • [4] Synthesis of ZnO nanorods by one step microwave-assisted hydrothermal route for electronic device applications
    N. Senthilkumar
    E. Vivek
    M. Shankar
    M. Meena
    M. Vimalan
    I. Vetha Potheher
    [J]. Journal of Materials Science: Materials in Electronics, 2018, 29 : 2927 - 2938
  • [5] Synthesis of ZnO nanorods by one step microwave-assisted hydrothermal route for electronic device applications
    Senthilkumar, N.
    Vivek, E.
    Shankar, M.
    Meena, M.
    Vimalan, M.
    Potheher, I. Vetha
    [J]. JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2018, 29 (04) : 2927 - 2938
  • [6] Microwave-assisted solid-state synthesis of ZnO nanorods
    Liu Jin-Song
    Cao Jie-Ming
    Li Zi-Quan
    Ke Xing-Fei
    [J]. ACTA CHIMICA SINICA, 2007, 65 (15) : 1476 - 1480
  • [7] Iodine-Catalyzed Mono- and Disulfenylation of Indoles in PEG400 through a Facile Microwave-Assisted Process
    Rahaman, Rajjakfur
    Barman, Pranjit
    [J]. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2017, 2017 (42) : 6327 - 6334
  • [8] Microwave-assisted hydrothermal synthesis and characterization of hierarchical structured ZnO nanorods
    Liu, H.
    Yang, D.
    Sun, H.
    Zhu, Z.
    [J]. JOURNAL OF OPTOELECTRONICS AND ADVANCED MATERIALS, 2010, 12 (10): : 2063 - 2068
  • [9] Microwave-assisted synthesis of silver nanorods
    Fu-Ken Liu
    Pei-Wen Huang
    Yu-Cheng Chang
    Fu-Hsiang Ko
    Tieh-Chi Chu
    [J]. Journal of Materials Research, 2004, 19 : 469 - 473
  • [10] Microwave-assisted synthesis of silver nanorods
    Liu, FK
    Huang, PW
    Chang, YC
    Ko, FH
    Chu, TC
    [J]. JOURNAL OF MATERIALS RESEARCH, 2004, 19 (02) : 469 - 473