Calix[4]arenequinazolinones. Synthesis and structure

被引：8

作者：

Rodik, R. ^{[1
]}

Rozhenko, A. B. ^{[1
,2
]}

Boyko, V. ^{[1
]}

Pirozhenko, V. V. ^{[1
]}

Danylyuk, O. ^{[3
]}

Suwinska, K. ^{[3
]}

Lipkowski, J. ^{[3
]}

Kalchenko, V. ^{[1
]}

机构：

[1] Natl Acad Sci Ukraine, Inst Organ Chem, UA-02660 Kiev, Ukraine

[2] Univ Bielefeld, D-33615 Bielefeld, Germany

[3] Polish Acad Sci, Inst Phys Chem, PL-01224 Warsaw, Poland

来源：

TETRAHEDRON | 2007年 / 63卷 / 46期

关键词：

D O I：

10.1016/j.tet.2007.08.047

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The synthesis of calix[4]arenes bearing two quinazolin-4-ones group at the upper rim is decribed. H-1 NMR spectra and quantum chemical calculations make it possible to suggest that calix[4]arenequinazolinones form three rotamers in solutions at room temperature, due to the restricted rotation of the quinazolinone fragments. The X-ray structure investigation indicates that quinazolin-4-onecalix[4]arene exists in the crystal state as the methanol 1: 1 inclusion complex. (C) 2007 Elsevier Ltd. All rights reserved.

引用

页码：11451 / 11457

页数：7

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