Non-destructive analysis of silver selenide films obtained by Pulsed Laser Deposition (PLD) with Micro-XRF

被引：6

作者：

Dargel, Rainer

Azeroual, Mohamed

Mogwitz, Boris

Janek, Juergen

Vogt, Carla

机构：

[1] Leibniz Univ Hannover, Inst Inorgan Chem, Dept Analyt Chem, D-30167 Hannover, Germany

[2] Univ Giessen, Inst Phys Chem, D-35392 Giessen, Germany

来源：

JOURNAL OF MATERIALS SCIENCE | 2007年 / 42卷 / 17期

关键词：

D O I：

10.1007/s10853-006-1310-2

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

Thin films of silver selenide with varying composition have been deposited on magnesium oxide substrates with pulsed laser deposition and were investigated via micro-XRF. A calibration procedure was designed to determine the absolute thicknesses of the films. The lateral homogeneity was investigated by elemental mapping, thus delivering information about the deposition process. Wet chemical analysis was performed on the dissolved layers with ICP-OES and ICP-MS to determine the stoichiometry of the Ag (x) Se (y) . The results suggest a correlation between the composition of the layers and their thicknesses by showing a silver enrichment for thinner layers.

引用

页码：7375 / 7380

页数：6

共 16 条

[1] Non-destructive analysis of silver selenide films obtained by Pulsed Laser Deposition (PLD) with Micro-XRF
Rainer Dargel
Mohamed Azeroual
Boris Mogwitz
Juergen Janek
Carla Vogt
[J]. Journal of Materials Science, 2007, 42 : 7375 - 7380
[2] Non-invasive and non-destructive micro-XRF and micro-Raman analysis of a decorative wallpaper from the beginning of the 19th century
Castro, Kepa
Perez-Alonso, Maite
Rodriguez-Laso, Maria Dolores
Etxebarria, Nestor
Madariaga, Juan Manuel
[J]. ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2007, 387 (03) : 847 - 860
[3] Non-invasive and non-destructive micro-XRF and micro-Raman analysis of a decorative wallpaper from the beginning of the 19th century
Kepa Castro
Maite Pérez-Alonso
María Dolores Rodríguez-Laso
Nestor Etxebarria
Juan Manuel Madariaga
[J]. Analytical and Bioanalytical Chemistry, 2007, 387 : 847 - 860
[4] In-situ non- destructive analysis of Etruscan gold jewels with the micro-XRF transportable spectrometer from CNA
Scrivano, S.
Ruberto, C.
Gomez-Tubio, B.
Mazzinghi, A.
Ortega-Feliu, I.
Ager, F. J.
Laclavetine, K.
Giuntini, L.
Respaldiza, M. A.
[J]. JOURNAL OF ARCHAEOLOGICAL SCIENCE-REPORTS, 2017, 16 : 185 - 193
[5] XPS Analysis of ZnO thin Films Obtained by Pulsed Laser Deposition
He, Jianting
Tan, Boxue
Su, Yuanbin
Yang, Shulian
Wei, Qinqin
[J]. MANUFACTURING SCIENCE AND TECHNOLOGY, PTS 1-8, 2012, 383-390 : 6293 - 6296
[6] Micro X-ray Florescence (μXRF):: A new analytical method for non-destructive mineral analysis
Cox, R. A.
Savard, D.
[J]. GEOCHIMICA ET COSMOCHIMICA ACTA, 2008, 72 (12) : A187 - A187
[7] Micro-invasive approach for non-destructive XRF analysis on light matrix: inside the Opus Lemovicense
Bonizzoni, Letizia
Galli, Anna
Riccardi, Maria Pia
Maggioni, Chiara
[J]. X-RAY SPECTROMETRY, 2015, 44 (03) : 169 - 176
[8] Micro-Raman study of nanocomposite porous films with silver nanoparticles prepared using pulsed laser deposition
Strelchuk, V. V.
Kolomys, O. F.
Golichenko, B. O.
Boyko, M. I.
Kaganovich, E. B.
Krishchenko, I. M.
Kravchenko, S. O.
Lytvyn, O. S.
Manoilov, E. G.
Nasieka, Iu. M.
[J]. SEMICONDUCTOR PHYSICS QUANTUM ELECTRONICS & OPTOELECTRONICS, 2015, 18 (01) : 46 - 52
[9] Approaching non-destructive surface chemical analysis of CMSX-4 superalloy with double-pulsed laser induced breakdown spectroscopy
McDonald, Joel P.
Das, Dipak K.
Nees, John A.
Pollock, Tresa M.
Yallsove, Steven M.
[J]. SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY, 2008, 63 (05) : 561 - 565
[10] Characterization of the new mobile confocal micro X-ray fluorescence (CXRF) system for in situ non-destructive cultural heritage analysis at the CNA: μXRF-CONCHA
Laclavetine, Kilian
Ager, Francisco J.
Arquillo, Joaquin
Angel Respaldiza, Miguel
Scrivano, Simona
[J]. MICROCHEMICAL JOURNAL, 2016, 125 : 62 - 68

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