An uncertainty spreadsheet for the k0-standardisation method in Neutron Activation Analysis

被引:5
|
作者
D'Agostino, G. [1 ]
Di Luzio, M. [1 ]
Oddone, M. [1 ,2 ]
机构
[1] Univ Pavia, Ist Nazl Ric Metrol INRIM, Dept Chem, Unit Radiochem & Spect, Via Taramelli 12, I-27100 Pavia, Italy
[2] Univ Pavia, Dept Chem, Via Taramelli 12, I-27100 Pavia, Italy
关键词
k(0)-standardisation method; Uncertainty budget; Spreadsheet technique; Correlated input quantities; Cerebrospinal fluid; REACTOR; K(0)-NAA;
D O I
10.1007/s10967-018-6094-8
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
This paper focuses on the use of the spreadsheet technique to set up the uncertainty budget for the k(0)-standardisation method in Neutron Activation Analysis. The adopted measurement model included most of presently recognized error sources and was written to limit the covariances between input quantities. The calculations were implemented in a worksheet file and tested in a multi-elemental analysis of a biological material. Besides, it was demonstrated that the k(0)-standardisation turns to the relative-standardisation when the monitor element corresponds to the analyte element. The developed worksheet is available and suitable for the analysis of other materials in different experimental conditions.
引用
收藏
页码:1261 / 1269
页数:9
相关论文
共 50 条
  • [1] An uncertainty spreadsheet for the k0-standardisation method in Neutron Activation Analysis
    G. D’Agostino
    M. Di Luzio
    M. Oddone
    Journal of Radioanalytical and Nuclear Chemistry, 2018, 318 : 1261 - 1269
  • [2] The k0-INRIM software: a tool to compile uncertainty budgets in neutron activation analysis based on k0-standardisation
    D'Agostino, G.
    Di Luzio, M.
    Oddone, M.
    MEASUREMENT SCIENCE AND TECHNOLOGY, 2020, 31 (01)
  • [3] The k0-INRIM software: a tool to compile uncertainty budgets in neutron activation analysis based on k0-standardisation (vol 31, 017002, 2020)
    D'Agostino, G.
    Di Luzio, M.
    Oddone, M.
    MEASUREMENT SCIENCE AND TECHNOLOGY, 2020, 31 (04)
  • [4] Utilization of k0-standardisation method of neutron activation analysis for determining the major and trace elements of medicinal plants from the Senhaja Srair region of Morocco
    I. Aarab
    H. Bounouira
    E. Chakir
    H. Amsil
    A. Didi
    Journal of Radioanalytical and Nuclear Chemistry, 2023, 332 : 3431 - 3443
  • [5] Utilization of k0-standardisation method of neutron activation analysis for determining the major and trace elements of medicinal plants from the Senhaja Srair region of Morocco
    Aarab, I.
    Bounouira, H.
    Chakir, E.
    Amsil, H.
    Didi, A.
    JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY, 2023, 332 (08) : 3431 - 3443
  • [6] Overall measurement uncertainty of k0-based neutron activation analysis
    Smodis, B.
    Bucar, T.
    JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY, 2006, 269 (02) : 311 - 316
  • [7] Overall measurement uncertainty of k0-based neutron activation analysis
    B. Smodiš
    T. Bučar
    Journal of Radioanalytical and Nuclear Chemistry, 2006, 269 : 311 - 316
  • [8] Application of the k0 method in neutron activation analysis and in prompt gamma activation analysis
    Revay, Zs
    Kennedy, G.
    RADIOCHIMICA ACTA, 2012, 100 (8-9) : 687 - 698
  • [9] Validation of a neutron activation analysis method using k0-standardization
    Acharya, RN
    Nair, AGC
    Reddy, AVR
    Manohar, SB
    APPLIED RADIATION AND ISOTOPES, 2002, 57 (03) : 391 - 398
  • [10] APPLICATION OF THE K(0) STANDARDIZATION METHOD IN NEUTRON-ACTIVATION ANALYSIS OF CERAMIC MATERIALS
    DARDENNE, C
    DESCHAMPS, N
    REVEL, G
    RIGLET, G
    HERVIOU, C
    JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY-ARTICLES, 1993, 168 (02): : 417 - 427