SYNTHESIS AND CHARACTERIZATION OF Fe3O4@MELAMINE SULFONIC ACID NANOCOMPOSITE AS A NOVEL MAGNETICALLY RECYCLABLE NANO CATALYST IN ONE-POT PREPARATION OF 3, 4-DIHYDROPYRIMIDINONES/THIONES

被引：0

作者：

Abdollahi, Narges ^{[1
]}

Kiasat, Ali Reza ^{[1
]}

Saghanezhad, Seyyed Jafar ^{[2
]}

机构：

[1] Shahid Chamran Univ, Dept Chem, Fac Sci, Ahvaz 6135743169, Iran

[2] ACECR Prod Technol Res Inst, Ahvaz, Iran

来源：

REVUE ROUMAINE DE CHIMIE | 2016年 / 61卷 / 03期

关键词：

nano catalyst; magnetically recyclable; nanocomposite; biginelli reaction; dihydropyrimidin-2(1H)-ones; BIGINELLI REACTION; REUSABLE CATALYST; NANOPARTICLES; EFFICIENT; GREEN; 3,4-DIHYDROPYRIMIDIN-2(1H)-ONES; POLYMER;

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Melamine sulfonic acid supported Fe3O4 magnetic nanocomposite, Fe3O4@MSA, has been prepared and successfully applied as a solid acid catalyst for one-pot three-component condensation reaction of aldehyde, beta-ketoester and urea or thiourea under solvent free conditions. The nanocomposite has been characterized by FT-ER, TGA and SEM spectroscopies. The nanomagnetic catalyst could be readily separated via application of an external magnet, allowing straightforward recovery and reuse.

引用

页码：159 / 167

页数：9

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