Determination of melamine in milk powder using gas chromatography-high-resolution isotope dilution mass spectrometry

被引：19

作者：

Koh, Guiwan ^{[1
]}

Chia, Rosalind S. C. ^{[1
]}

Lin, Qi ^{[1
]}

Cheow, Pui-Sze ^{[1
]}

Teo, Tang-Lin ^{[1
]}

Lee, Tong-Kooi ^{[1
]}

机构：

[1] Capricorn, Hlth Sci Author, Chem Metrol Div, Chem Metrol Lab, Singapore 117528, Singapore

来源：

JOURNAL OF SEPARATION SCIENCE | 2011年 / 34卷 / 21期

关键词：

GC; High resolution isotope dilution MS; Melamine; Milk powder; PERFORMANCE LIQUID-CHROMATOGRAPHY; CYANURIC ACID; DAIRY-PRODUCTS; PET FOOD; RESIDUES; EGG;

D O I：

10.1002/jssc.201100285

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A GC-high-resolution isotope dilution MS (IDMS) method for the quantification of melamine in milk powder is described. The developed technique is compared to the LC-IDMS/MS technique, typically used for the determination of melamine in various matrices. The accuracy of the GC-high-resolution IDMS method was demonstrated when a small degree of equivalence was obtained in a regional comparative study involving the determination of melamine in milk powder.

引用

页码：3043 / 3052

页数：10

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