Preparation and characterization of novel glass-ceramic tile with microwave absorption properties from iron ore tailings

被引:45
|
作者
Yao, Rui [1 ]
Liao, SongYi [1 ]
Dai, ChangLu [2 ]
Liu, YuChen [1 ]
Chen, XiaoYu [1 ]
Zheng, Feng [1 ,3 ]
机构
[1] Cent S Univ, Sch Mat Sci & Engn, Changsha 410083, Hunan, Peoples R China
[2] Guangdong Bode Fine Bldg Mat Co Ltd, Foshan 528000, Peoples R China
[3] Cent S Univ, Phase Diagrams & Mat Design Ctr, Changsha 410083, Hunan, Peoples R China
关键词
Glass ceramics; Magnetic properties; Cation distribution; Microwave absorption properties; RAY-DIFFRACTION PATTERNS; QUANTITATIVE INTERPRETATION; MAGNETIC-PROPERTIES; DIELECTRIC-PROPERTIES; ELECTRICAL-TRANSPORT; FERRITE; PERMEABILITY; SPECTRA; IONS; MIXTURES;
D O I
10.1016/j.jmmm.2014.11.066
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A novel glass-ceramic tile consisting of one glass-ceramic layer (GC) attaining microwave absorption properties atop ceramic substrate was prepared through quench-heat treatment route derived from iron ore tailings (IOTs) and commercial raw materials (purity range 73-99%). X-ray diffraction (XRD), SEM, Energy dispersive X-ray spectroscopy (EDS), Fourier transform infrared spectroscopy (FTIR), Physical property measurement system (PPMS) and Vector network analyzer (VNA) measurements were carried out to investigate phase, microstructure, magnetic and microwave absorption aspects of the glass-ceramic layer. Roughly 806 +/- 1.7 wt% borosilicate glass and 194 +/- 1.7 wt% spinel ferrite with chemical formula of (Zn0.172+Fe0.833+)[Fe1.173+Fe0.062+Ni0.772+]O-4 were found among the tested samples. Absorption of Electromagnetic wave by 3 mm thick glass-ceramic layer at frequency of 2-18 GHz reached peak reflection loss (RL) of -17.61 dB (98.27% microwave absorption) at 10.31 GHz. Altering the thickness of the glass-ceramic layer can meet the requirements of different level of microwave absorption. (C) 2014 Elsevier B.V. All rights reserved
引用
收藏
页码:367 / 375
页数:9
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