Determination of acetone in cow's raw milk by flow injection and gas chromatographic methods

被引:0
|
作者
Baticz, O [1 ]
Vida, L [1 ]
Tömösközi, S [1 ]
机构
[1] Budapest Univ Technol & Econ, Dept Biochem & Food Technol, H-1111 Budapest, Hungary
关键词
acetone; flow injection analysis; gas chromatography; ketone bodies;
D O I
暂无
中图分类号
TS2 [食品工业];
学科分类号
0832 ;
摘要
An automatic flow injection (FIA) and two possible reference gas chromatographic (liquid and headspace sampling GC) methods including appropriate sample preparation were developed and validated for determination of acetone in milk. The methods were tested by preserved raw milk samples. The FIA results were compared with data obtained by GC determinations. It was found that FIA procedure is suitable for rapid automated measurement of acetone in the range of 0-5 mmol l(-1) in milk, therefore it is a promising analytical method for ketosis monitoring in dairy farms.
引用
收藏
页码:297 / 311
页数:15
相关论文
共 50 条
  • [1] Gas chromatographic determination of organochlorine pesticides in cow milk
    Armendáriz, C
    de Ciriza, JAP
    Farré, R
    INTERNATIONAL JOURNAL OF FOOD SCIENCES AND NUTRITION, 2004, 55 (03) : 215 - 221
  • [2] Fluorescence microscopy methods for the determination of somatic cell count in raw cow's milk
    Zajac, P.
    Zubricka, S.
    Capla, J.
    Zelenakova, L.
    VETERINARNI MEDICINA, 2016, 61 (11) : 612 - 622
  • [3] Evaluation of flow injection analysis for determination of urea in sheep's and cow's milk
    Baumgartner, M
    Flöck, M
    Winter, P
    Luf, P
    Baumgartner, W
    ACTA VETERINARIA HUNGARICA, 2002, 50 (03) : 263 - 271
  • [4] Determination of Protein Content of Raw Fresh Cow's Milk Using Dielectric Spectroscopy Combined with Chemometric Methods
    Zhu, Xinhua
    Guo, Wenchuan
    Kang, Fei
    Kong, Fanrong
    Zhu, Qiang
    FOOD AND BIOPROCESS TECHNOLOGY, 2016, 9 (12) : 2092 - 2102
  • [5] Determination of Protein Content of Raw Fresh Cow’s Milk Using Dielectric Spectroscopy Combined with Chemometric Methods
    Xinhua Zhu
    Wenchuan Guo
    Fei Kang
    Fanrong Kong
    Qiang Zhu
    Food and Bioprocess Technology, 2016, 9 : 2092 - 2102
  • [7] Liquid chromatographic determination of tylosin in mastitic cow's milk following therapy
    Dudriková, E
    Jozef, S
    Jozef, N
    JOURNAL OF AOAC INTERNATIONAL, 1999, 82 (06) : 1303 - 1307
  • [8] Fluoroquinolone Residues in Raw Cow's Milk
    Navratilova, Pavlina
    Borkovcova, Ivana
    Vyhnalkova, Jana
    Vorlova, Lenka
    CZECH JOURNAL OF FOOD SCIENCES, 2011, 29 (06) : 641 - 646
  • [9] A GAS-CHROMATOGRAPHIC HEADSPACE METHOD FOR THE DETERMINATION OF ACETONE IN BOVINE-MILK, BLOOD AND URINE
    WINTERBACH, HEK
    APPS, PJ
    ONDERSTEPOORT JOURNAL OF VETERINARY RESEARCH, 1991, 58 (02) : 75 - 79
  • [10] A COMPARISON OF CHROMATOGRAPHIC METHODS FOR DETERMINATION OF S-TRIAZINES IN MILK
    HAJSLOVA, J
    RYPAROVA, L
    VIDEN, I
    DAVIDEK, J
    KOCOUREK, V
    ZEMANOVA, I
    INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1990, 38 (02) : 105 - 114