Morphology control of hydroxyapatite through hydrothermal process

被引:90
|
作者
Zhu, Ronghai [1 ,2 ]
Yu, Ranbo [3 ]
Yao, Jianxi [1 ]
Wang, Dan [1 ]
Ke, Jiajun [1 ]
机构
[1] Chinese Acad Sci, Inst Proc Engn, Key Lab Multiphase React, Beijing 100080, Peoples R China
[2] Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China
[3] Univ Sci & Technol Beijing, Dept Phys Chem, Beijing 100083, Peoples R China
基金
中国国家自然科学基金;
关键词
hydroxyapatite; morphology; hexagonal prism;
D O I
10.1016/j.jallcom.2007.03.081
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Hexagonal hydroxyapatite (HAP) has been successfully synthesized by using EDTA as chelate under hydrothermal condition. The as-prepared samples were characterized by SEM and XRD. The XRD result indicated that the products were preferentially oriented along c-axis. The SEM photographs showed that the size of the crystals was well controlled by the reaction parameters such as temperature, pH value, reaction time and the mole ratio of EDTA/Ca. (C) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码:555 / 559
页数:5
相关论文
共 50 条
  • [1] Morphology Control of Hydroxyapatite as a Potential Reinforcement for Orthopedic Biomaterials: The Hydrothermal Process
    Szterner, Piotr
    Antosik, Agnieszka
    Pagacz, Joanna
    Tymowicz-Grzyb, Paulina
    CRYSTALS, 2023, 13 (05)
  • [2] Hydroxyapatite morphology control by hydrothermal treatment
    Kawachi, G.
    Ishida, E. H.
    Ioku, K.
    BIOCERAMICS, VOL 19, PTS 1 AND 2, 2007, 330-332 : 103 - +
  • [3] An Effective Morphology Control of Hydroxyapatite Crystals via Hydrothermal Synthesis
    Neira, Ines S.
    Kolen'ko, Yury V.
    Lebedev, Oleg I.
    Van Tendeloo, Gustaaf
    Gupta, Himadri S.
    Guitian, Francisco
    Yoshimura, Masahiro
    CRYSTAL GROWTH & DESIGN, 2009, 9 (01) : 466 - 474
  • [4] Controlling morphology of hydroxyapatite nanoparticles through hydrothermal microemulsion chemical synthesis
    Garcia, Carlos
    Garcia, Claudia
    Paucar, Carlos
    INORGANIC CHEMISTRY COMMUNICATIONS, 2012, 20 : 90 - 92
  • [5] The morphology control of hydroxyapatite microsphere at high pH values by hydrothermal method
    Qi, Yongcheng
    Shen, Juan
    Jiang, Qiying
    Jin, Bo
    Chen, Jiwei
    Zhang, Xia
    ADVANCED POWDER TECHNOLOGY, 2015, 26 (04) : 1041 - 1046
  • [6] Morphology control of PbS nanocrystals by a novel hydrothermal process
    Ji, YJ
    Yang, DR
    Zhang, H
    Ma, XY
    Xu, J
    Que, DL
    FUNCTIONAL NANOMATERIALS FOR OPTOELECTRONICS AND OTHER APPLICATIONS, 2004, 99-100 : 197 - 201
  • [7] Hydrothermal synthesis and morphology variation of cadmium hydroxyapatite
    Zhu, K
    Yanagisawa, K
    Onda, A
    Kajiyoshi, K
    JOURNAL OF SOLID STATE CHEMISTRY, 2004, 177 (12) : 4379 - 4385
  • [8] Tubular hydroxyapatite formation through a hydrothermal process from α-tricalcium phosphate with anatase
    Kamitakahara, Masanobu
    Takahashi, Hiroko
    Ioku, Koji
    JOURNAL OF MATERIALS SCIENCE, 2012, 47 (09) : 4194 - 4199
  • [9] Tubular hydroxyapatite formation through a hydrothermal process from α-tricalcium phosphate with anatase
    Masanobu Kamitakahara
    Hiroko Takahashi
    Koji Ioku
    Journal of Materials Science, 2012, 47 : 4194 - 4199
  • [10] Hierarchically nanostructured hydroxyapatite: hydrothermal synthesis, morphology control, growth mechanism, and biological activity
    Ma, Ming-Guo
    INTERNATIONAL JOURNAL OF NANOMEDICINE, 2012, 7 : 1781 - 1791