Synthesis, Characterization and Magnetic Properties of Nickel Ferrite by Soft Chemical Method

被引：3
|
作者：
Ghosh, Sushmita [1 ]
Dasgupta, Subrata [1 ]
机构：
[1] Cent Glass & Ceram Res Inst, CSIR, Ceram Membrane Div, Kolkata 700032, India
来源：
TRANSACTIONS OF THE INDIAN CERAMIC SOCIETY | 2010年 / 69卷 / 01期
关键词：
Nanopowder; Magnetic properties; Soft chemical method; Phase analysis; Powder Processing; REVERSE MICELLE TECHNIQUE; NANOCRYSTALLINE NICKEL; SPINEL FERRITES; ROUTE; PARTICLES; POWDERS;
D O I：
10.1080/0371750X.2010.11090817
中图分类号：
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Synthesis of nanosized nickel ferrite by a template method where tartaric acid is used as a ligand and nitric acid as an oxidant is described. The synthesized powders were characterized by TGA, XRD, FTIR, TEM, BET, VSM and SQUID studies. The average crystallite size of the phase pure material was of 30 nm and the surface area was found to be 20.37 m(2).g(-1). Magnetic measurements of the phase pure powder were carried out at room temperature by VSM at a magnetic field of 1 Tesla, and by SQUID at a magnetic field of 6 Tesla. High saturation magnetization of 31.43 emu.g(-1) is observed in case of VSM and 43.36 emu.g(-1) is observed for SQUID measurements. Comparative analysis of M-s values synthesized by different routes are compared.
引用
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页码：25 / 28
页数：4
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