Synthesis and rheological study of some maleic acid and fumaric acid stereoregular polyesters, 10 -: Synthesis and characterization of α,ω-dihydroxyoligo(alkylene maleate)s

被引：0
|
作者：
Dunjic, B
Sepulchre, MO
Sepulchre, M
Spassky, N
Djonlagic, J
机构：
[1] Univ Paris 06, Lab Chim Macromol, URA 24, F-75252 Paris 05, France
[2] Univ Belgrade, Fac Technol & Met, YU-11001 Belgrade, Yugoslavia
来源：
MACROMOLECULAR CHEMISTRY AND PHYSICS | 1998年 / 199卷 / 06期
关键词：
D O I：
10.1002/(SICI)1521-3935(19980601)199:6<1051::AID-MACP1051>3.3.CO;2-#
中图分类号：
O63 [高分子化学（高聚物）];
学科分类号：
070305 ; 080501 ; 081704 ;
摘要：
alpha,omega-Dihydroxyoligo(alkylene maleate)s with molecular weights ranging from 1500 to 4000 were prepared by polycondensation, in 1-methyl-2-pyrrolidone at 105 degrees C, of potassium maleate and 1,4-dibromobutane, 1,6-dibromohexane or 1,8-dibromooctane in the presence of 2-bromoethanol. The structure of oligomers was checked by H-1 and C-13 NMR spectroscopy. In most cases the mean functionality of oligomers is reasonably close to two.
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页码：1051 / 1055
页数：5
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