3-(Trimethylsilyl)prop-2-ynyl p-toluenesulfonate

被引：0
|
作者：
Schmitt, Devin C. [1 ]
Morales, Guillermo A. [1 ]
Fronczek, Frank R. [1 ]
Watkins, Steven F. [1 ]
机构：
[1] Louisiana State Univ, Dept Chem, Baton Rouge, LA 70803 USA
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
D O I：
10.1107/S1600536811043595
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C13H18O3SSi, the SO3 group displays a partial rotational (ca 50 degrees) disorder about the C-S bond, with relative proportions 0.7744 (13):0.2256 (13). This disorder also forces the propynyl CH2 group to be disordered.
引用
收藏
页码：O3110 / U2086
页数：9
相关论文
共 50 条
  • [1] Prop-2-ynyl 3-(3,4-dihydroxyphenyl)-prop-2-enoate monohydrate
    Xia, CN
    Zhou, W
    Hu, WX
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1783 - O1784
  • [2] Tris(prop-2-ynyl)ammonium chloride
    Steiner, T
    Schreurs, AMM
    Kroon, J
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 1156 - 1158
  • [3] A LEWIS ACID MEDIATED REARRANGEMENT OF 1-(TRIMETHYLSILYL)PROP-2-YNYL TRIMETHYLSILYL ETHERS TO 2-TRIMETHYLSILYL ENONES
    ENDA, J
    KUWAJIMA, I
    JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1984, (23) : 1589 - 1590
  • [4] 3-(Benzothiazol-2-yl)-3-(prop-2-ynyl)hex-5-yn-2-one
    Baryala, Yamna
    Zerzouf, Abdelfettah
    Salem, Moussa
    Essassi, El Mokhtar
    El Ammari, Lahcen
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O857 - U2527
  • [5] Tris(prop-2-ynyl)ammonium chloride
    Steiner, Thomas
    Schreurs, Antoine M. M.
    Kroon, Jan
    Acta Crystallographica, Section C: Crystal Structure Communications, 1999, 55 (07): : 1156 - 1158
  • [6] REACTIONS OF CHLOROCYCLOPENTADIENES WITH PROP-2-YNYL BROMIDE AND BROMOALLENE
    ALEXANDER, R
    DAVIES, DI
    JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1971, (01): : 5 - +
  • [7] Prop-2-ynyl as a protective group for carboxylic acids: A mild method for the highly selective deprotection of prop-2-ynyl esters using tetrathiomolybdate
    Ilankumaran, P
    Manoj, N
    Chandrasekaran, S
    CHEMICAL COMMUNICATIONS, 1996, (16) : 1957 - 1958
  • [8] Synthesis and biological evaluation of 3-(prop-2-enyl)- and 3-(prop-2-ynyl)pyrrolidine-2,5-dione derivatives as potential aromatase inhibitors
    Barrell, KJ
    Woo, WL
    Ahmadi, M
    Smith, HJ
    Nicholls, PJ
    JOURNAL OF PHARMACY AND PHARMACOLOGY, 1996, 48 (02) : 154 - 159
  • [9] ALLENES .1. THE REARRANGEMENT OF PROP-2-YNYL ACETATES
    LANDOR, PD
    LANDOR, SR
    JOURNAL OF THE CHEMICAL SOCIETY, 1956, (APR): : 1015 - 1019
  • [10] SYNTHESIS OF 3-OCTYL-3-(PROP-2-YNYL)PYRROLIDINE-2,5-DIONE, 3-CYCLOHEXYLMETHYL-3-(PROP-2-YNYL)PYRROLIDINE-2,5-DIONE AND 3-CARBOXY-3-(PROP-2-YNYL)PYRROLIDINE-2,5-DIONES REQUIRED AS POTENTIAL AROMATASE INHIBITORS
    WOO, LWL
    SMITH, HJ
    BARRELL, KJ
    NICHOLLS, PJ
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1993, (21): : 2549 - 2553
12345