Ceric ion initiation of methyl methacrylate from poly(glycidyl azide)-diol

被引：26

作者：

Arslan, H

Eroglu, MS

Hazer, B ^{[1
]}

机构：

[1] Zonguldak Karaelmas Univ, Dept Chem, TR-67100 Zonguldak, Turkey

[2] TUBITAK, Marmara Res Ctr, Dept Chem, TR-41470 Kocaeli, Turkey

[3] Food Sci & Technol Res Inst, TR-41470 Kocaeli, Turkey

来源：

EUROPEAN POLYMER JOURNAL | 2001年 / 37卷 / 03期

关键词：

redox initiation; ceric ammonium nitrate; poly(methyl methacrylate)-b-poly(glycidyl azide); tetrabutyl ammonium hydrogen sulphate;

D O I：

10.1016/S0014-3057(00)00126-9

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

Polymerization of methyl methacrylate initiated by eerie ammonium nitrate in combination with poly(glycidyl azide)-diol was investigated in aqueous nitric acid. Poly(methyl methacrylate)-b-poly(glycidyl azide) copolymer was obtained. Block copolymer yield was increased using tetrabutyl ammonium hydrogen sulphate as a surfactant. The effect of nitric acid, eerie ions and diol concentration on the block copolymer yield was investigated. Block copolymers were characterized using GPC,H-1-NMR, FTIR, DSC, TGA and fractional precipitation methods. (C) 2001 Elsevier Science Ltd. All rights reserved.

引用

页码：581 / 585

页数：5

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