Determination of carbendazim and thiabendazole in environmental water by solid phase extraction and high performance liquid chromatography

被引：0

作者：

Guo, YN ^{[1
]}

Jiang, ZS ^{[1
]}

Zhang, M ^{[1
]}

Feng, LJ ^{[1
]}

Zhao, JY ^{[1
]}

Li, JC ^{[1
]}

机构：

[1] NE Normal Univ, Fac Chem, Changchun 130024, Peoples R China

来源：

CHINESE JOURNAL OF ANALYTICAL CHEMISTRY | 2005年 / 33卷 / 03期

关键词：

high performance liquid chromatography; solid phase extraction; carbendazim; thiabendazole; fungicide;

D O I：

暂无

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

A reversed phase high performance liquid chromatographic (HPLC) method for the separation and determination of trace concentrations of carbendazim, ( MBC) and thiabendazole ( TBZ) in water was introduced. Water was subjected to solid-phase extraction ( SPE) using C-18 cartridge. The analytical column of HPLC was Hypersil ODS with a mobile phase of methanol-water (50:50, VIV) at a flow rate of 0. 7 mUmin, temperature of column at 55 degrees C and wavelength at 286 nm. The method is simple, rapid, accurate, and precise. It has satisfactory repeatability and recovery. Limit of detection is about 0. 05 mg/L.

引用

页码：395 / 397

页数：3

共 7 条

[1] Analysis of carbendazim, benomyl, thiophanate methyl and 2,4-dichlorophenoxyacetic acid in fruits and vegetables after supercritical fluid extraction
Anastassiades, M
Schwack, W
[J]. JOURNAL OF CHROMATOGRAPHY A, 1998, 825 (01) : 45 - 54
[2] DETERMINATION OF CARBENDAZIM IN BLUEBERRIES BY REVERSED-PHASE HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY
BUSHWAY, RJ
HURST, HL
KUGABALASOORIAR, J
PERKINS, LB
[J]. JOURNAL OF CHROMATOGRAPHY, 1991, 587 (02): : 321 - 324
[3] COLINGE A, 1983, J CHROMATOGR, V257, P416
[4] DETERMINATION AND CONFIRMATION OF BENOMYL AND CARBENDAZIM IN WATER USING HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHY AND DIODE-ARRAY DETECTION
DHOOT, JS
DELROSARIO, AR
[J]. JOURNAL OF CHROMATOGRAPHY, 1993, 645 (01): : 178 - 181
[5] FEI YC, 1985, CONCISE PESTICIDE DI
[6] MARVIN CH, 1994, J CHROMATOGR, V555, P147
[7] LIQUID-CHROMATOGRAPHIC DETERMINATION OF CARBENDAZIM IN THE PRESENCE OF SOME NORMAL SOIL CONSTITUENTS WITH PHOTODIODE-ARRAY DETECTION
SANCHEZRASERO, F
ROMERO, TE
DIOS, CG
[J]. JOURNAL OF CHROMATOGRAPHY, 1991, 538 (02): : 480 - 483

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