Microstructure and Mechanical Properties of a High-Mn TWIP Steel Subjected to Cold Rolling and Annealing

The structure-property relationship was studied in an Fe-18Mn-0.6C-1.5Al steel subjected to cold rolling to various total reductions from 20% to 80% and subsequent annealing for 30 min at temperatures of 673 to 973 K. The cold rolling resulted in significant strengthening of the steel. The hardness increased from 1900 to almost 6000 MPa after rolling reduction of 80%. Recovery of cold worked microstructure developed during annealing at temperatures of 673 and 773 K, resulting in slight softening, which did not exceed 0.2. On the other hand, static recrystallization readily developed in the cold rolled samples with total reductions above 20% during annealing at 873 and 973 K, leading to fractional softening of about 0.8. The recrystallized grain size depended on annealing temperature and rolling reduction; namely, it decreased with a decrease in the temperature and an increase in the rolling reduction. The mean recrystallized grain size from approximately 1 to 8 m could be developed depending on the rolling/annealing conditions. The recovered and fine grained recrystallized steel samples were characterized by improved strength properties. The yield strength of the recovered, recrystallized, and partially recrystallized steel samples could be expressed by a unique relationship taking into account the fractional contributions from dislocation and grain size strengthening into overall strength.