HALOCYCLIZATION OF 3-ALLYLTHIO-5H-[1,2,4]TRIAZINO[5,6-b]INDOLE

被引：9

作者：

Kim, D. G. ^{[1
]}

Zhuravlyova, A. V. ^{[1
]}

机构：

[1] S Urals State Univ, Chelyabinsk 454080, Russia

来源：

CHEMISTRY OF HETEROCYCLIC COMPOUNDS | 2010年 / 46卷 / 07期

关键词：

3-allylthio-5H-[1,2,4]triazino[5,6-b]indole; 3-halomethyl-3,10-dihydro-2H-[1,3]thiazolo[3 ',2 ':2,3][1,2,4]triazino[5,6-b]indolium halides; phase-transfer catalysis; one-pot synthesis;

D O I：

10.1007/s10593-010-0599-6

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The synthesis of 3-allylthio-5H-[1,2,4]triazino[5,6-b]indole has been carried out by the reaction of 3-mercapto-5H-[1,2,4]triazino[5,6-b]indole with allyl bromide in the NaOH-H(2)O-DMSO system and in a one-pot synthesis from isatin-beta-thiosemicarbazide. Halocyclization of allylthio-5H-[1,2,4]triazino[5,6-b]indole synthesized the 3-halomethyl-3,10-dihydro-2H-[1,3]thiazolo[3',2':2,3][1,2,4]triazino[5,6-b]indolium halides.

引用

页码：896 / 898

页数：3

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