Synthesis and crystal structure of (±)-1-[(2-hydroxy-5-methylphenyl) (phenyl)methyl]-2-pyridylbenzimidazole

被引:0
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作者
Wang, JY
Zhou, J
Cheng, DL [1 ]
Jian, PM
Zhang, GL
机构
[1] Lanzhou Univ, Dept Chem, Lanzhou 730000, Peoples R China
[2] Yangzhou Univ, Dept Chem, Yangzhou 225002, Peoples R China
[3] Chinese Acad Sci, Chengdu Inst Biol, Chengdu 610041, Peoples R China
来源
关键词
(+/-)-benzimidazole; synthesis; crystal structure;
D O I
暂无
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
(+/-)-1-[(2-Hydroxy-5-methylphenyl) (phenyl) methyl]-2-pyridylbenzimidazole was synthesized and its crystal structure was determined by X-ray four-cycle diffraction method. The crystal belongs to monoclinic, space group P2(1)/c, with the crystal cell parameters: a=1.351 4(5) nm, b=0.965 9(6) nm, c=1.674 0(3) nm, beta =110.2 7(2)degrees, V=2.049 7(14) nm(3), Z=4, D-c=1.269 g/cm(3), R-1 = 0.057 5. The analyses of crystal structure show that the chain structure is formed by intermolecular H-bond.
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页码:1861 / 1863
页数:3
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