(2R,3aS,5aR,8aR,8bS)-4-Bromo-2-(4methoxyphenyl)-7,7-dimethyl-3a,5a,8a,8b-tetrahydrobenzo[1,2-d:3,4-d′]bis[1,3]dioxole

被引：2

作者：

Banwell, Martin G. ^{[1
]}

Kokas, Okanya J. ^{[1
]}

Willis, Anthony C. ^{[1
]}

机构：

[1] Australian Natl Univ, Res Sch Chem, Inst Adv Studies, Canberra, ACT 0200, Australia

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2007年 / 63卷

关键词：

D O I：

10.1107/S1600536807039232

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C17H19BrO5, bears an exo-orientated or R-configured 4-methoxyphenyl group and incorporates a C - O bond that is distinctly shorter than the three remaining acetal C - O bonds [1.415 (4) versus 1.431 (4) - 1.448 (4) angstrom and 1.421 (4) versus 1.436 (4) - 1.448 (4) angstrom for the two molecules in the asymmetric unit].

引用

页码：O3820 / U3116

页数：15

共 50 条

[1] [(3aS,5aR,8aR,8bS)-2,2,7,7-Tetramethyltetrahydro-3aH-bis[1,3]dioxolo[4,5-b:4 ',5 '-d]pyran-3a-yl]methyl (R)-N-(1-phenylethyl)sulfamate
Xie, Meng
Shen, Si-Si
Chen, Bao-Feng
Sha, Yu
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1581 - +
[2] 2R, 3aS, 8aR)-2-(4-methoxyphenyl)3,3a, 8,8a-tetrahydro-2H-indeno[1,2-d]oxazole
Uchida, Akira
Hattori, Tetsutaro
Yamaura, Masanori
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O420 - O421
[3] Crystal structure, Hirshfeld surface analysis and corrosion inhibition study of 3,6-bis(pyridin-2-yl)-4-{[(3aS,5aR,8aR,8bS)-2,2,7,7-tetrametbyltetra-hydro-5H-bis[1,3]dioxolo[4,5-b:4′,5′-d]pyran-5-yl)-methoxy]methyl}pyriaazine monohydrate
Filali, Mouad
Elmsellem, Hicham
Hokelek, Tuncer
El-Ghayoury, Abdelkrim
Stetsiuk, Oleh
El Hadrami, El Mestafa
Ben-Tama, Abdessalam
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2019, 75 : 1169 - +
[4] (5aR,8aR,9R)-9-(3,4,5-trimethoxyphenyl)5a,6,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxole-5,8-dione
Shi, JF
Wang, YG
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2003, 59 : O756 - O758
[5] (3aS,5aR,6R,8aR)-3a-hydroxy-5a-methyl-6-[(1R,2E,4R)-1,4,5-trimethyl-2-hexen-1-yl]-3a,4,5,5a,6,7,8,8a-octahydro-2H-cyclopenta[e]benzofuran-2-one
Wang, Wen-Liang
Tao, Hong-Wen
Sun, Wei
Gu, Qian-Qun
Zhu, Wei-Ming
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O4196 - U2258
[6] (3aR,3bS,4aR,4bR,5aR,5bS)-4,4,8,8-tetra-bromo-2,2-dimethylperhydrodicyclopropa-[e,g][1,3]benzodioxole-3b-carbonitrile
Banwell, MG
Forman, GS
Hockless, DCR
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1996, 52 : 1804 - 1806
[7] (5R,5aR,8aR,9S)-5-(3,4-dihydroxy-5-methoxyphenyl)-9-fluoro-5,8,8a,9-tetrahydrofuro[3′,4′: 6,7]naphtho[2,3-d]-1,3-dioxol-6(5aH)-one acetone solvate
Zhou, FY
Jian, SZ
He, XY
Wang, YG
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1374 - O1376
[8] (1R,4bS,8aR)-(1,2,3,4b,5,6,7,8,8a,9a-Decahydro-4,9a-diazafluoren-1-yl)-methanol
Kooijman, H
Spek, AL
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 2000, 56 : E295 - E296
[9] Crystal structure and DFT calculations of 3,8-diphenyl-3a,4,5,5a,8a,8b-hexahydro-benzo [1,2-d:3,4-d′]diisoxazole, C20H18N2O2
Bovio, B
Caramella, P
Quadrelli, P
JOURNAL OF MOLECULAR STRUCTURE, 2005, 743 (1-3) : 135 - 143
[10] (+)-(2R,8aR*)-[(8,8-dimethoxycamphoryl)sulfonyl]oxaziridine and (+)-(2R,8aR*)-[(8,8-dichlorocamphoryl)sulfonyl]oxaziridine - ([4H-4a,7-methanooxazirino[3,2-i][2,1]benzisothiazole, tetrahydro-8,8-dimethoxy-9,9-dimethyl-, 3,3-dioxide], [2R-(2 alpha,4a alpha,7 alpha,8aR*)]- and [4H-4a,7-methanooxazirino[3,2-i][2,1]benzisothiazole, 8,8-dichlorotetrahydro-9,9-dimethyl-, 3,3-dioxide,[2R-(2 alpha,4a alpha,7 alpha,8aR*)])
Chen, BC
Murphy, CK
Kumar, A
Reddy, RT
Clark, C
Zhou, P
Lewis, BM
Gala, D
Mergelsberg, I
Scherer, D
Buckley, J
DiBenedetto, D
Davis, FA
ORGANIC SYNTHESIS, VOL 73, 1996, 73 : 159 - 173

← 1 2 3 4 5 →