Three-dimensional reconstruction of a nickel-alumina composite coating by FIB-SIMS

被引：3
|
作者：
Chater, Richard J. [1 ]
Corni, Ilaria [1 ]
Boccaccini, Aldo R. [1 ]
Ryan, Mary P. [1 ]
机构：
[1] Univ London Imperial Coll Sci Technol & Med, Dept Mat, London SW7 2AZ, England
来源：
SURFACE AND INTERFACE ANALYSIS | 2011年 / 43卷 / 1-2期
关键词：
nickel coating; alumina particle; SIMS imaging; FIB-SIMS; 3D reconstruction; ELECTRODEPOSITION; NANOPARTICLES; RESISTANCE; PARTICLES;
D O I：
10.1002/sia.3453
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
The alumina particle distribution in a nickel-alumina composite coating on stainless steel was determined using the aluminum secondary ion images that were generated by sputtering a cross-section of the coating with a highly focused gallium primary ion beam(FIB). Thin slices of the coating were removed using the same beam with further imaging of the fresh surface which was very smooth despite the difference in the sputter rates of the two materials. Sequential SIMS imaging and sectioning resulted in a sequence of images from which the 3D distribution of the alumina particles in the composite coating was reconstructed. Copyright (C) 2010 John Wiley & Sons, Ltd.
引用
收藏
页码：492 / 494
页数：3
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