Study on parameters optimization of silver nanoparticles biosynthesized using aqueous extract of Imperata cylindrica

被引:3
|
作者
Bonnia, Noor Najmi [1 ]
Ab Rani, Mohd Azri [2 ]
Fairuzi, Afiza Ahmad [1 ]
机构
[1] Univ Teknol MARA, Fac Appl Sci, Sch Phys & Mat Sci, Shah Alam 40460, Selangor, Malaysia
[2] Univ Teknol MARA, Fac Appl Sci, Sch Chem & Environm, Shah Alam 40460, Selangor, Malaysia
关键词
Biosynthesis; Silver nanoparticles; Imperata cylindrica; Optimization; Monodisperse; GREEN SYNTHESIS; SIZE; GOLD; TEMPERATURE;
D O I
10.5004/dwt.2020.24856
中图分类号
TQ [化学工业];
学科分类号
0817 ;
摘要
Biosynthesis of nanoparticles has gained great attention in moving towards an economic and environmentally friendly process. However, there is a limited number of studies that describe the parameters for tuning the dimension and geometry of nanoparticles in the biosynthesis process. Therefore, in this study, silver nanoparticles were synthesized by varying the synthesis parameters in aqueous extract of Imperata cylindrica. The particles were characterized by visual observation; color changes, UV-visible spectroscopy, dynamic light scattering, field scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction. Changing the parameters such as plant extract concentration, silver salt concentration, the temperature of biosynthesis and pH of reaction mixture influence the size and dispersion of the nanoparticles. The optimum parameters for synthesizing silver nanoparticles are 10% of aqueous extract, 10 mM of silver nitrate, pH 5.7 with a reaction temperature of 60 degrees C. The synthesized silver nanoparticles are in spherical with a diameter below 100 nm.
引用
收藏
页码:186 / 195
页数:10
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