System maps for retention of neutral organic compounds under isocratic conditions on a reversed-phase monolithic column

被引：24

作者：

Chu, Y ^{[1
]}

Poole, CF ^{[1
]}

机构：

[1] Wayne State Univ, Dept Chem, Detroit, MI 48202 USA

来源：

JOURNAL OF CHROMATOGRAPHY A | 2003年 / 1003卷 / 1-2期

关键词：

retention properties; monoclinic columns; system maps; organic compounds; neutral;

D O I：

10.1016/S0021-9673(03)00845-8

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The solvation parameter model is used to create systems maps for the separation of neutral organic compounds on a Chromolith Performance RP-18e octadecylsiloxane-bonded silica-based monolithic column for water-acetonitrile and water-methanol mobile phase compositions from 10 to 70% (v/v) organic solvent. These results demonstrate that the retention properties of the monolithic column are similar to those of conventional octadecylsiloxane-bonded silica particle-packed columns. It is further shown that the selectivity for the monolithic column falls within the selectivity range for typical particle-packed columns at two mobile phase compositions for which a direct comparison is possible. (C) 2003 Elsevier B.V. All rights reserved.

引用

页码：113 / 121

页数：9

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