Growth and morphology of mesoporous SBA-15 particles

被引：100
|
作者：
Linton, Peter [1 ]
Alfredsson, Viveka [1 ]
机构：
[1] Lund Univ, SE-22100 Lund, Sweden
来源：
CHEMISTRY OF MATERIALS | 2008年 / 20卷 / 09期
关键词：
D O I：
10.1021/cm703375p
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
A study was conducted to analyze the growth progression of mesoporous silica particles with the SBA-15 structure. The analysis aimed to study the dynamic of the micellar aggregation and its effects on the particular growth and particle size. SBA-15 was synthesized with Pluronic P104 as structure director and with HCI as the acid medium. Tetramethyl orthosilicate (TMOS) was used to get silica for synthesis. TMOS and other reagents were mixed and tempered to the specified temperature for getting accurate synthesis results. Transmission electron microscope was used to record electron micrographs on carbon copper grids. The nucleation process was performed to obtain a monodisperse size distribution of the silica particles. The growth of particles was observed on the synthesis temperatures. Results show that the synthesis protocol offers an easy way of making highly-structured SBA-15 with well-defined particle size.
引用
收藏
页码：2878 / 2880
页数：3
相关论文
共 50 条
  • [1] A study of morphology of mesoporous silica SBA-15
    Chao, MC
    Lin, HP
    Sheu, HS
    Mou, CY
    [J]. NANOPOROUS MATERIALS III, 2002, 141 : 387 - 394
  • [2] Investigation of the morphology of the mesoporous SBA-16 and SBA-15 materials
    Stevens, WJJ
    Lebeau, K
    Mertens, M
    Van Tendeloo, G
    Cool, P
    Vansant, EF
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2006, 110 (18): : 9183 - 9187
  • [3] Morphology-selective synthesis of mesoporous SBA-15 particles over micrometer, submicrometer and nanometer scales
    Lee, Hyung Ik
    Kim, Jin Hoe
    Stucky, Galen D.
    Shi, Yifeng
    Pak, Chanho
    Kim, Ji Man
    [J]. JOURNAL OF MATERIALS CHEMISTRY, 2010, 20 (39) : 8483 - 8487
  • [4] Controlling particle morphology and size in the synthesis of mesoporous SBA-15 materials
    Linton, Peter
    Wennerstrom, Hakan
    Alfredsson, Viveka
    [J]. PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2010, 12 (15) : 3852 - 3858
  • [5] Tuning Textural Properties by Changing the Morphology of SBA-15 Mesoporous Materials
    da Silva, Francisco Emanuel
    Rigoti, Eduardo
    de Mello, Mariele Iara Soares
    Pergher, Sibele B. C.
    [J]. MATERIALS, 2024, 17 (12)
  • [6] Adsorption of octadecyltrichlorosilane on mesoporous SBA-15
    Mirji, S. A.
    Halligudi, S. B.
    Sawant, Dhanashri P.
    Jacob, Nalini E.
    Patil, K. R.
    Gaikwad, A. B.
    Pradhan, S. D.
    [J]. APPLIED SURFACE SCIENCE, 2006, 252 (12) : 4097 - 4103
  • [7] Adsorption of methanol on mesoporous SBA-15
    Mirji, S. A.
    Halligudi, S. B.
    MatheW, Nevin
    Jacob, Nalini E.
    Patil, K. R.
    Gaikwad, A. B.
    [J]. MATERIALS LETTERS, 2007, 61 (01) : 88 - 92
  • [8] SBA-15 templated-ordered mesoporous carbon: effect of SBA-15 microporosity
    Yang, Y
    Sayari, A
    [J]. NANOPOROUS MATERIALS IV, 2005, 156 : 543 - 550
  • [9] SBA-15 templated mesoporous carbon: New insights into the SBA-15 pore structure
    Sayari, A
    Yang, Y
    [J]. CHEMISTRY OF MATERIALS, 2005, 17 (24) : 6108 - 6113
  • [10] Structure sensitivity of vibrational spectra of mesoporous silica SBA-15 and Pt/SBA-15
    Borodko, Y
    Ager, JW
    Marti, GE
    Song, H
    Niesz, K
    Somorjai, GA
    [J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2005, 109 (37): : 17386 - 17390
12345