Synthesis of inorganic fullerene-like MoS2 nanoparticles by a facile method

被引：16
|
作者：
Du, Kai [1 ]
Fu, Wuyou [1 ]
Wei, Ronghui [1 ]
Yang, Haibin [1 ]
Liu, Shikai [1 ]
Yu, Shidan [1 ]
Zou, Guangtian [1 ]
机构：
[1] Jilin Univ, Natl Lab Superhand Mat, Changchun 130012, Jilin, Peoples R China
来源：
MATERIALS LETTERS | 2007年 / 61卷 / 27期
关键词：
fullerenes; nanomaterials; MoS2; hollow cage; ammonium molybdate;
D O I：
10.1016/j.matlet.2007.03.071
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
A facile and low-cost synthesis route was used to synthesize inorganic fullerene-like (IF) MoS2 nanoparticles by reaction of sulfur powder and ammonium molybdate in a hydrogen atmosphere at 600 degrees C. As-synthesized IF-MoS2 nanoparticles are of a closed hollow cage structure with size of 10-20 nm. Nanowires and nanotubes were also obtained at the same annealing temperature. The composition, structure, and morphology of the products were characterized by XRD, Raman, and TEM and the possible growth mechanism is proposed. (c) 2007 Elsevier B.V. All rights reserved.
引用
收藏
页码：4887 / 4889
页数：3
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