One-step synthesis of tenorite (CuO) nano-particles from Cu4 (SO4) (OH) 6 by direct thermal-decomposition method

被引:65
|
作者
Bakhtiari, Fereshteh [2 ,3 ]
Darezereshki, Esmaeel [1 ]
机构
[1] Shahid Bahonar Univ Kerman, Energy & Environm Engn Res Ctr, Kerman, Iran
[2] Shahid Bahonar Univ Kerman, Mineral Ind Res Ctr, Kerman, Iran
[3] Shahid Bahonar Univ Kerman, Dept Chem Engn, Kerman, Iran
关键词
Brochantite; Chemical synthesis; Decomposition; Nano-particles; Powder technology; Tenorite; NANOPARTICLES; COPPER;
D O I
10.1016/j.matlet.2010.09.071
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this research work, CuO nano-particles were synthesized at 750 degrees C (for 2 h) by the direct thermal-decomposition method using the brochantite as precursor. The nano-particles were characterized using X-ray diffraction (XRD), energy dispersive spectra (EDS), infrared spectrum (IR), and scanning electron microscope (SEM). SEM image showed that the CuO nano-particles were of rod shape with diameter and length of 235 +/- 5 nm and 856 +/- 5 nm, respectively. As a result, this method could be used at an industrial scale as a cheap and convenient way in production of pure tenorite nano-particles. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码:171 / 174
页数:4
相关论文
共 8 条
  • [1] Synthesis, characterization, and thermal decomposition kinetics of copper hydroxide sulfate (Cu4(SO4)(OH)6) synthesized by chemical precipitation method
    Guner, Eda Keles
    Kancan, Duygu
    Naktiyok, Jale
    ozer, Abdulkadir
    [J]. ASIA-PACIFIC JOURNAL OF CHEMICAL ENGINEERING, 2021, 16 (01)
  • [2] One-step synthesis of hematite (α-Fe2O3) nano-particles by direct thermal-decomposition of maghemite
    Darezereshki, Esmaeel
    [J]. MATERIALS LETTERS, 2011, 65 (04) : 642 - 645
  • [3] One-step Synthesis of CoFe2O4 Nano-particles by Mechanical alloying
    Rashidi, Sedigheh
    Ataie, Abolghasem
    [J]. ULTRAFINE GRAINED AND NANO-STRUCTURED MATERIALS IV, 2014, 829 : 747 - 751
  • [4] Synthesis and characterization of novel nanostructured fishbone-like Cu(OH)2 and CuO from Cu4SO4(OH)6
    Jia, Wenzhao
    Reitz, Eliot
    Sun, Hui
    Zhang, Heng
    Lei, Yu
    [J]. MATERIALS LETTERS, 2009, 63 (05) : 519 - 522
  • [5] Catalyst-free synthesis of ZnO-CuO-ZnFe2O4 nanocomposites by a rapid one-step thermal decomposition approach
    Al-Gaashani, R.
    Aissa, B.
    Hossain, Md Anower
    Radiman, S.
    [J]. MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING, 2019, 90 : 41 - 49
  • [6] TG-DTA-MS STUDIES ON THE THERMAL-DECOMPOSITION BEHAVIOR OF HOMOGENEOUSLY PRECIPITATED ZR2(SO4)(OH)6-CENTER-DOT-6H2O
    LU, CW
    SHI, JL
    XI, TG
    YANG, XH
    CHEN, YX
    [J]. THERMOCHIMICA ACTA, 1994, 232 (01) : 77 - 84
  • [7] One-step thermal decomposition of C4H4FeO6 to Fe3O4@carbon nano-composite for high-performance lithium-ion batteries
    Xu, Leilei
    Jiao, Ranran
    Tao, Xuquan
    Yi, Xiujie
    Wei, Denghu
    [J]. MATERIALS CHEMISTRY AND PHYSICS, 2020, 239
  • [8] One-step synthesis of nano-hydroxyapatite/graphene nanosheet hybrid coatings on Ti6Al4V alloys by hydrothermal method and their in-vitro corrosion responses
    Yigit, Oktay
    Dikici, Burak
    Senocak, Taha Cagri
    Ozdemir, Niyazi
    [J]. SURFACE & COATINGS TECHNOLOGY, 2020, 394 (394):