5-Methoxy-3-[(5-methoxy-1H-indol-3-yl)(phenyl)methyl]-1H-indole

被引：2
|
作者：
Narayanan, P. [1 ]
Sethusankar, K. [1 ]
Ramachandiran, K. [2 ]
Perumal, P. T. [2 ]
机构：
[1] RKM Vivekananda Coll Autonomous, Dept Phys, Madras 600004, Tamil Nadu, India
[2] Cent Leather Res Inst, Div Organ Chem, Madras 600020, Tamil Nadu, India
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
data-to-parameter ratio = 11.7; mean σ(C-C) = 0.003 Å; R factor = 0.041; single-crystal X-ray study; T = 293 K; wR factor = 0.119;
D O I：
10.1107/S1600536811045491
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C25H22N2O2, the indole rings are individually almost planar [with maximum deviations of 0.0116 (19) and 0.0113 (18) angstrom] and are almost orthogonal to each other, making a dihedral angle of 84.49 (6)degrees. The benzene ring is inclined at 72.83 (9) and 80.85 (9)degrees with respect to the indole rings. In the crystal, molecules are linked by N-H center dot center dot center dot O interactions into chains running parallel to the c axis. The crystal structure is further stabilized by C-H center dot center dot center dot pi interactions.
引用
收藏
页码：O3196 / U2049
页数：11
相关论文
共 50 条
  • [1] 5-Methoxy-1-[(5-methoxy-1H-indol-2-yl)methyl]-1H-indole
    Attia, Mohamed I.
    El-Brollosy, Nasser R.
    Ghabbour, Hazem A.
    Arshad, Suhana
    Fun, Hoong-Kun
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O971 - +
  • [2] (5-Methoxy-1H-indol-3-yl)acetonitrile
    Ge, Yu-Hua
    Li, Jin-Feng
    Luo, Yang-Hui
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : O66 - +
  • [3] Methyl 4-(5-methoxy-1H-indol-3-yl)benzoate
    Wang, Cui-Ping
    Yu, Jiang-Long
    Zhang, Zhi-Qiang
    Yan, Jing-Bo
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68
  • [4] 5-Methoxy-2-[(5-methoxy-1H-indol-1-yl)carbonyl]-1H-indole
    Attia, Mohamed I.
    El-Brollosy, Nasser R.
    Ei-Emam, Ali A.
    Ng, Seik Weng
    Tiekink, Edward R. T.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O1775 - +
  • [5] N-Cyclohexyl-2-(5-methoxy-1H-indol-3-yl)-2-oxoacetamide
    Liu, Jing
    Liu, Yong-Feng
    Zhang, Shi
    Gao, Ying
    Chen, Hong
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O288 - U2137
  • [6] Vibrational and electronic profiles, molecular docking and biological prediction of 5-methoxy-1-[(5-methoxy-1H- indol-2-yl) methyl]-1H-indole: Experimental and theoretical investigations
    Haress, Nadia G.
    Manimaran, Devarasu
    Joe, Isaac Hubert
    EL-Azzouny, Aida A.
    Al-Wabli, Reem I.
    Attia, Mohamed I.
    [J]. JOURNAL OF THEORETICAL & COMPUTATIONAL CHEMISTRY, 2016, 15 (06):
  • [7] Ethyl 3,3,3-trifluoro-2-hydroxy-2-(5-methoxy-1H-indol-3-yl)propionate
    Kadirova, Zukhra
    Tolipov, Samat
    Fedorovskiy, Oleg
    Bakhtiyar, Ibragimov
    Parpiev, Nusrat
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1619 - U2300
  • [8] 4-Desoxy-4β-[(5-methoxy-1H-indol-3-yl)oxalylamino]podophyllotoxin methanol solvate
    Feng, Min
    Zhao, Ming
    Zhang, Jingze
    Yang, Zaixin
    Chen, Hong
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O2339 - U2361
  • [9] 5-Methoxy-1-(3,4,5-trimethoxyphenyl)-1H-indole
    Monroe, Thomas Blake
    Rimland, Casey
    Moazami, Yasamin
    Jones, Daniel S.
    Ogle, Craig A.
    [J]. ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1678 - U358
  • [10] 3-Chloro-4-(5-methoxy-1H-indol-3-yl)cyclobut-3-ene-1,2-dione
    Duc Hoang Lande
    Messal, Marleen
    Reimann, Vincent
    Renger, Caren
    Rurka, Constanze
    Schoemaker, Jana
    Schroeder, Nadin K.
    Gruenefeld, Johann
    [J]. MOLBANK, 2013, (03)
12345